2,3-DIMETHYLDECANE

Base Information

• Chemical Name: 2,3-DIMETHYLDECANE
• CAS No.: 17312-44-6
• Molecular Formula: C₁₂H₂₆
• Molecular Weight: 170.338
• Hs Code.: 2901100000
• Mol file: 17312-44-6.mol

Synonyms:2,3-Dimethyldecane;

Chemical Property of 2,3-DIMETHYLDECANE

Chemical Property:

• Vapor Pressure: 0.315mmHg at 25°C
• Melting Point: -50.8°C (estimate)
• Refractive Index: 1.42
• Boiling Point: 208 °C at 760 mmHg
• Flash Point: 139.2 °C
• PSA: 0.00000
• Density: 0.749 g/cm³
• LogP: 4.63900

Purity/Quality:

98% ^*data from raw suppliers

2,3-Dimethyldecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,F
• Hazard Codes: Xi,F

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIMETHYLDECANE

There total 4 articles about 2,3-DIMETHYLDECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyl bromide (507-19-7) + oct-1-ene (111-66-0,25068-25-1) → 2,3-Dimethyl-decan (17312-44-6)

Guidance literature:

With bis(cyclopentadienyl)titanium dichloride; triethylaluminum; In hexane; at 20 - 22 ℃; for 12h;

DOI:10.1023/A:1016088918435

Reference yield:

→ (-)-2,3-dimethyl-decane (17312-44-6)

Guidance literature:

With methyl magnesium iodide; diethyl ether; anschl. Dehydratisierung mit Oxalsaeure und katalytische Hydrierung in Eisessig an PtO₂ bei 1.75 at Druck;

Reference yield:

3-methyl-butan-2-one (563-80-4) + n-heptylmagnesium bromide (13125-66-1) → 2,3-Dimethyl-decan (17312-44-6)

Guidance literature:

With diethyl ether; Erhitzen des Reaktionsprodukts mit Aluminiumoxid auf 280grad und Hydrieren des Olefin-Gemisches an Raney-Nickel bei 150grad/100 at;

upstream raw materials:

3-methyl-butan-2-one

n-heptylmagnesium bromide

t-butyl bromide

oct-1-ene

Refernces