Sulfurous diamide, tetramethyl-

Base Information

• Chemical Name: Sulfurous diamide, tetramethyl-
• CAS No.: 3768-60-3
• Molecular Formula: C4H12N2OS
• Molecular Weight: 136.218
• European Community (EC) Number: 223-201-7
• DSSTox Substance ID: DTXSID30191112
• Nikkaji Number: J217.666A
• Wikidata: Q83063601
• Mol file: 3768-60-3.mol

Synonyms:Sulphinylbis(dimethylamide);3768-60-3;EINECS 223-201-7;AI3-50899;Sulfurous diamide, tetramethyl-;Tetramethyl sulfurous diamide;Sulfinylbis(dimethylamine);tetramethylsulphurous diamide;tetramethyl-sulfurous diamide;C4H12N2OS;SCHEMBL9291076;SULFINYLBIS(DIMETHYLAMIDE);DTXSID30191112;N,N,N',N'-Tetramethylsulfurousdiamide;N,N,N',N'-tetramethylsulfurous diamide

Chemical Property of Sulfurous diamide, tetramethyl-

Chemical Property:

• Vapor Pressure: 0.208mmHg at 25°C
• Boiling Point: 209°Cat760mmHg
• Flash Point: 80.2°C
• Density: 1.148g/cm³
• XLogP3: 0.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 136.06703418
• Heavy Atom Count: 8
• Complexity: 82

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)S(=O)N(C)C

Technology Process of Sulfurous diamide, tetramethyl-

There total 5 articles about Sulfurous diamide, tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

bis(dimethylamino)sulfide (2129-20-6) → N,N,N',N'-tetramethylsulfurous acid diamine (3768-60-3)

Guidance literature:

With tert-butylhypochlorite; triethylamine; In Petroleum ether; at -30 ℃;

Reference yield:

dimethyl amine (124-40-3) → N,N,N',N'-tetramethylsulfurous acid diamine (3768-60-3)

Guidance literature:

With thionyl chloride; at -78 ℃;

DOI:10.1021/ja01630a056

Reference yield:

tri(dimethylamino)arsenic (6596-96-9) → N,N,N',N'-tetramethylsulfurous acid diamine (3768-60-3)

Guidance literature:

With sulfur dioxide; In diethyl ether;

DOI:10.1246/bcsj.51.1481

upstream raw materials:

dimethyl amine

bis(dimethylamino)sulfide

tri(dimethylamino)arsenic

tetrakis(dimethylamino)titanium

Downstream raw materials:

N,N-dimethyltriphenylmethylamine

1-Dimethylamino-1,3-diphenyl-2-propen

dimethyl-amidosulfurous acid-chloride

(dimethylamino)di-n-propylborane

Refernces

• 1、 Fay, Laurent B.,Newton, Anthony,Simian, Herve,Robert, Fabien,Douce, David,Hancock, Peter,Green, Martin,Blank, Imre. "Potential of gas chromatography-orthogonal acceleration time-of-flight mass spectrometry (GC-oaTOFMS) in flavor research". . p. 2708 - 2713. Retrieved 2007/10/03.