Technology Process of Octylphosphonic acid
There total 24 articles about Octylphosphonic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hypophosphorous acid; palladium; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
water; N,N-dimethyl-formamide;
at 110 ℃;
for 24h;
DOI:10.1080/10426507.2012.727925
- Guidance literature:
-
1-bromo-octane;
With
aluminum (III) chloride; triethyl phosphite;
at 20 - 160 ℃;
for 7h;
With
hydrogen bromide;
In
water;
for 5h;
Reagent/catalyst;
Temperature;
Reflux;
- Guidance literature:
-
With
trifluorormethanesulfonic acid;
In
toluene;
at 100 ℃;
for 24h;
Sealed tube;
Schlenk technique;
Inert atmosphere;
DOI:10.1021/acs.joc.0c00550
