N-chlorosulfonyl dicyclohexylamine

Base Information

• Chemical Name: N-chlorosulfonyl dicyclohexylamine
• CAS No.: 99700-74-0
• Molecular Formula: C₁₂H₂₂ClNO₂S
• Molecular Weight: 279.831
• Mol file: 99700-74-0.mol

Synonyms:Sulfamoylchloride, dicyclohexyl- (6CI,9CI); N-Chlorosulfonyldicyclohexylamine;N-Dicyclohexylamine sulfonyl chloride

Chemical Property of N-chlorosulfonyl dicyclohexylamine

Chemical Property:

• Vapor Pressure: 3.08E-06mmHg at 25°C
• Boiling Point: 388.4°Cat760mmHg
• Flash Point: 188.7°C
• PSA: 45.76000
• Density: 1.22g/cm³
• LogP: 4.51820

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-chlorosulfonyl dicyclohexylamine

There total 2 articles about N-chlorosulfonyl dicyclohexylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexyl-chloroamine (22824-16-4) → dicyclohexyl-sulfamoyl chloride (99700-74-0)

Guidance literature:

With tetrachloromethane; sulfur dioxide; chlorine;

Reference yield:

→ dicyclohexyl-sulfamoyl chloride (99700-74-0)

Guidance literature:

SO2Cl2, Dicyclohexylamin;

DOI:10.1002/9780470132395.ch29

Reference yield: 65.0%

dicyclohexyl-sulfamoyl chloride (99700-74-0) + (S,S)-1,2-diaminocyclohexane (21436-03-3) → (1S,2S)-N-(N,N-dicyclohexylsulfamoyl)-1,2-cyclohexanediamine

Guidance literature:

In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/S0957-4166(02)00659-6

upstream raw materials:

dicyclohexyl-chloroamine