DI-N-BUTOXYBORYLBENZENE

Base Information

• Chemical Name: DI-N-BUTOXYBORYLBENZENE
• CAS No.: 7330-48-5
• Molecular Formula: C14H23BO2
• Molecular Weight: 234.146
• Mol file: 7330-48-5.mol

Synonyms:Benzeneboronicacid, dibutyl ester (6CI,7CI,8CI);Dibutoxyphenylborane;Dibutylphenylboronate;NSC 526743;Phenyldibutoxyborane;

Chemical Property of DI-N-BUTOXYBORYLBENZENE

Chemical Property:

• Vapor Pressure: 0.00117mmHg at 25°C
• Refractive Index: 1.464
• Boiling Point: 309.4 °C at 760 mmHg
• Flash Point: 140.9 °C
• PSA: 18.46000
• Density: 0.91 g/cm³
• LogP: 3.01520

Purity/Quality:

98%min ^*data from raw suppliers

DI-N-BUTOXY BORYL BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DI-N-BUTOXYBORYLBENZENE

There total 29 articles about DI-N-BUTOXYBORYLBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(n-butyloxy)chloro-phenylborane (13029-25-9) + mercury(II) oxide (12653-71-3) → triphenylboroxine (3262-89-3) + dibutoxyphenylborane (7330-48-5)

Guidance literature:

In Petroleum ether; 0°C;

DOI:10.1016/0022-1902(68)80429-4

Reference yield:

hexaphenyl-1.2.4.5-tetraaza-3.6-diborane (13831-68-0) + butan-1-ol (71-36-3) → dibutoxyphenylborane (7330-48-5) + diphenyl hydrazine (122-66-7)

Guidance literature:

DOI:10.1039/j19660001590

Reference yield:

phenylborondichloride (873-51-8) → dibutoxyphenylborane (7330-48-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / benzene

2: light petroleum / Heating

With triethylamine; In Petroleum ether; benzene;

DOI:10.1039/j19660001590

upstream raw materials:

boric acid tributyl ester

triphenylboroxine

butan-1-ol

phenylborondichloride

Downstream raw materials:

2-(butyl-phenyl-boranyloxy)-ethylamine

2-[(1-methyl-heptyl)-phenyl-boranyloxy]-ethylamine

n-Butoxy-phenyl-(2,4,6-trimethylphenyl)-boran

2-phenyl-2,3-dihydrobenzo[d][1,3,2]diazaborinin-4(1H)-one

Refernces