1-iodobuta-1,3-diyne

Base Information

• Chemical Name: 1-iodobuta-1,3-diyne
• CAS No.: 6088-91-1
• Molecular Formula: C4HI
• Molecular Weight: 175.956
• Mol file: 6088-91-1.mol

Synonyms:

Chemical Property of 1-iodobuta-1,3-diyne

Chemical Property:

• Vapor Pressure: 7.18mmHg at 25°C
• Boiling Point: 141.9°Cat760mmHg
• Flash Point: 60.3°C
• Density: 2.186g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-iodobuta-1,3-diyne

There total 3 articles about 1-iodobuta-1,3-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetylene (74-86-2,25067-58-7) → acetylene-d1 (2210-34-6) + vinyliodide (593-66-8) + iodoacetylene (14545-08-5) + iododiacetylene (6088-91-1) + C2H(2)H*HI + deuteroiodoacetylene (14545-09-6)

Guidance literature:

With hydrogen iodide; deuterium iodide; at -261.2 ℃; for 6.7h; Mechanism; Irradiation; in solid krypton, variation of time;

DOI:10.1021/j100352a035

Reference yield:

butadiynediyl-bis-magnesium dibromide (38067-44-6) → iododiacetylene (6088-91-1) + 1,4-diiodo-1,3-diacetylene (53214-97-4)

Guidance literature:

With diethyl ether; iodine;

Reference yield:

→ iododiacetylene (6088-91-1)

Guidance literature:

J2 (2 Mol), Et2O, Diacetylen, Butyllithium, -80grad;

DOI:10.1016/0040-4020(66)80071-6

upstream raw materials:

butadiynediyl-bis-magnesium dibromide

acetylene

Downstream raw materials:

Butadiyne

1-iodopent-1-yne

Refernces