3,2'-dimethyl-4-nitrosobiphenyl

Base Information

• Chemical Name: 3,2'-dimethyl-4-nitrosobiphenyl
• CAS No.: 70786-64-0
• Molecular Formula: C₁₄H₁₃NO
• Molecular Weight: 211.263
• Mol file: 70786-64-0.mol

Synonyms:3,2'-Dimethyl-4-nitrosobiphenyl;

Chemical Property of 3,2'-dimethyl-4-nitrosobiphenyl

Chemical Property:

• Refractive Index: 1.5780 (estimate)
• Boiling Point: 331.2 °C at 760 mmHg
• Flash Point: 135.9 °C
• PSA: 29.43000
• Density: 1.05 g/cm³
• LogP: 4.36830

Purity/Quality:

99% ^*data from raw suppliers

3,2'-DIMETHYL-4-NITROSOBIPHENYL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,2'-dimethyl-4-nitrosobiphenyl

There total 1 articles about 3,2'-dimethyl-4-nitrosobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',3 dimethyl 4 aminobiphenyl (13394-86-0) → 3,2'-Dimethyl-4-nitroso-biphenyl (70786-64-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform;

DOI:10.1021/jm00194a019

Reference yield:

3,2'-Dimethyl-4-nitroso-biphenyl (70786-64-0) → N-(3,2'-Dimethyl-biphenyl-4-yl)-hydroxylamine (70786-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: MCPBA / CHCl₃

2: Zn

With 3-chloro-benzenecarboperoxoic acid; zinc; In chloroform;

DOI:10.1021/jm00194a019

upstream raw materials:

2',3 dimethyl 4 aminobiphenyl

Downstream raw materials:

N-(3,2'-Dimethyl-biphenyl-4-yl)-hydroxylamine

Refernces