DODECYLMETHANESULFONATE

Base Information

• Chemical Name: DODECYLMETHANESULFONATE
• CAS No.: 51323-71-8
• Molecular Formula: C13H28 O3 S
• Molecular Weight: 264.43
• Hs Code.: 2905199090
• Mol file: 51323-71-8.mol

Synonyms:1-(Methanesulfonyloxy)dodecane;1-Dodecyl mesylate; Dodecyl mesylate; Dodecyl methanesulfonate; Laurylmesylate; NSC 61860; n-Dodecyl methanesulfonate

Chemical Property of DODECYLMETHANESULFONATE

Chemical Property:

• Vapor Pressure: 2.28E-05mmHg at 25°C
• Boiling Point: 370.9°Cat760mmHg
• Flash Point: 178.1°C
• PSA: 51.75000
• Density: 0.977g/cm³
• LogP: 4.96430

Purity/Quality:

99.5% ^*data from raw suppliers

DODECYL METHANESULFONATE AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DODECYLMETHANESULFONATE

There total 6 articles about DODECYLMETHANESULFONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-dodecyl alcohol (112-53-8) + methanesulfonyl chloride (124-63-0) → dodecyl mesylate (51323-71-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 0.25h;

DOI:10.1002/chem.201300817

Reference yield: 94.0%

→ dodecyl mesylate (51323-71-8)

Guidance literature:

Reference yield:

2-(8-bromooctyloxy)tetrahydropyran (50816-20-1) → dodecyl mesylate (51323-71-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Li₂CuCl₄, 2.) PTSA / 1.) THF, room temperature, 12 h, 2.) CH₃OH, room temperature, 6 h

2: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

With pyridine; dilithium tetrachlorocuprate; toluene-4-sulfonic acid; In dichloromethane;

DOI:10.1039/P19940002849

upstream raw materials:

1-dodecyl alcohol

methanesulfonyl chloride

2-(8-bromooctyloxy)tetrahydropyran

1,8-Octanediol

Downstream raw materials:

ethyl tridecanoate

tridecanoic acid

2-(4-Cyanbenzyloxy)-1-dodecyloxy-3-(octadecyloxy)propan

dodecane

Refernces

• 1、 Rigo, Graziela Vargas,Trein, Márcia Rodrigues,da Silva Trentin, Danielle,Macedo, Alexandre José,de Oliveira, Bruno Assis,de Almeida, Angelina Maria,Giordani, Raquel Brandt,de Almeida, Mauro Vieira,Tasca, Tiana. "Diamine derivative anti-Trichomonas vaginalis and anti-Tritrichomonas foetus activities by effect on polyamine metabolism". . p. 847 - 855. Retrieved 2017/09/13.
• 2、 Paramanik, Minakshmi,Singh, Rekha,Mukhopadhyay, Sulekha,Ghosh, Sunil K.. "Catalytic nucleophilic fluorination by an imidazolium ionic liquid possessing trialkylphosphine oxide functionality". . p. 47 - 55. Retrieved 2015/07/15.