2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethyl acrylate

Base Information

• Chemical Name: 2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethyl acrylate
• CAS No.: 19812-60-3
• Molecular Formula: C11H20 O6
• Molecular Weight: 248.276
• Hs Code.: 2916129000
• European Community (EC) Number: 243-339-1
• DSSTox Substance ID: DTXSID10173532
• Nikkaji Number: J225.290B
• Wikidata: Q83043593
• Mol file: 19812-60-3.mol

Synonyms:19812-60-3;2-[2-[2-(2-HYDROXYETHOXY)ETHOXY]ETHOXY]ETHYL ACRYLATE;2-(2-(2-(2-Hydroxyethoxy)ethoxy)ethoxy)ethyl acrylate;EINECS 243-339-1;2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl prop-2-enoate;2-Propenoic acid, 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester;2-{2-[2-(2-HYDROXYETHOXY)ETHOXY]ETHOXY}ETHYL PROP-2-ENOATE;2-Propenoic acid, 2-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)ethyl ester;tetraethyleneglycol acrylate;SCHEMBL224782;DTXSID10173532;MFCD28145823;AKOS024258061;AS-72334;2-(2-(2-(2-Hydroxyethoxy)ethoxy)ethoxy)ethylacrylate;Propenoic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester

Chemical Property of 2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethyl acrylate

Chemical Property:

• Vapor Pressure: 3.43E-06mmHg at 25°C
• Boiling Point: 347°C at 760 mmHg
• PKA: 14.36±0.10(Predicted)
• Flash Point: 124.7°C
• PSA: 74.22000
• Density: 1.102g/cm³
• LogP: -0.24230
• XLogP3: -0.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 13
• Exact Mass: 248.12598835
• Heavy Atom Count: 17
• Complexity: 194

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC(=O)OCCOCCOCCOCCO

Technology Process of 2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethyl acrylate

There total 2 articles about 2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Tetraethylene glycol (112-60-7) + acryloyl chloride (814-68-6,25189-84-8) → tetraethylene glycol monoacrylate (19812-60-3,9051-31-4)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 52h;

DOI:10.1021/ma301833j

Reference yield: 51.0%

Tetraethylene glycol (112-60-7) + acrylic acid (79-10-7) → tetraethylene glycol monoacrylate (19812-60-3,9051-31-4)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 25h;

DOI:10.1021/la203829d

Reference yield: 90.0%

4-bromomethyl-3-nitrobenzoic acid (55715-03-2) + tetraethylene glycol monoacrylate (19812-60-3,9051-31-4) → C19H24BrNO9 (1355155-09-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 25h;

DOI:10.1021/la203829d

upstream raw materials:

Tetraethylene glycol

acryloyl chloride

acrylic acid

Downstream raw materials:

Acrylic acid 2-{2-[2-(2-iodo-ethoxy)-ethoxy]-ethoxy}-ethyl ester

C₃₁H₄₇NO₁₁

C₁₉H₂₄BrNO₉

((oxybis(ethane-2,1-diyl))bis(oxy))bis(ethane-2,1-diyl) diacrylate

Refernces

• 1、 Choi, U Hyeok,Mittal, Anuj,Price, Terry L.,Gibson, Harry W.,Runt, James,Colby, Ralph H.. "Polymerized ionic liquids with enhanced static dielectric constants". . p. 1175 - 1186. Retrieved 2013.
• 2、 -. "POLYMERS AND POLYMERIC NANOGELS WITH HYDROPHILICS ENCAPSULATION AND RELEASE CAPABILITIES AND METHODS THEREOF". Paragraph 0095; 0096; 0097. . Retrieved 2016/04/10.