1,1-Dicyclohexyldodecane

Base Information

• Chemical Name: 1,1-Dicyclohexyldodecane
• CAS No.: 18254-57-4
• Molecular Formula: C24H46
• Molecular Weight: 334.629
• DSSTox Substance ID: DTXSID80171303
• Nikkaji Number: J644.110F
• Wikidata: Q83041382
• Mol file: 18254-57-4.mol

Synonyms:1,1-Dicyclohexyldodecane;18254-57-4;1,1-dicyclohexyl-dodecane;DTXSID80171303

Chemical Property of 1,1-Dicyclohexyldodecane

Chemical Property:

• Boiling Point: 424.6°Cat760mmHg
• Flash Point: 200.2°C
• Density: 0.866g/cm³
• XLogP3: 11.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 12
• Exact Mass: 334.359951467
• Heavy Atom Count: 24
• Complexity: 252

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCC(C1CCCCC1)C2CCCCC2

Technology Process of 1,1-Dicyclohexyldodecane

There total 5 articles about 1,1-Dicyclohexyldodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-diphenyl-dodecane (1603-53-8) → 1,1-dicyclohexyl-dodecane (18254-57-4)

Guidance literature:

With nickel; at 150 ℃; under 73550.8 - 110326 Torr; Hydrogenation;

Reference yield:

cyclohexane (110-82-7,25012-93-5) + dodecylcyclohexane (1795-17-1) → 12-Methyl-tricosan (22331-52-8) + 1,1-dicyclohexyl-dodecane (18254-57-4)

Guidance literature:

With hydrogen; at 200 ℃; for 18h; under 37503.8 Torr; Reagent/catalyst; Temperature; Catalytic behavior;

DOI:10.1039/d1gc03350f

Reference yield:

ethyl laurate (106-33-2) → 1,1-dicyclohexyl-dodecane (18254-57-4)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erhitzen des Reaktionsprodukts mit Al₂O₃ auf 320grad/1 Torr und Hydrieren der erhaltenen Verbindung an Raney-Nickel bei 70grad/100-150 at

2: Raney nickel / 150 °C / 73550.8 - 110326 Torr / Hydrogenation

With diethyl ether; nickel;

upstream raw materials:

1,1-diphenyl-dodecane

ethyl laurate

cyclohexane

dodecylcyclohexane

Downstream raw materials:

1,1-diphenyl-dodecane

1-cyclohexyl-1-phenyl-dodecane

Refernces