N-benzoylaspartic acid

Base Information

• Chemical Name: N-benzoylaspartic acid
• CAS No.: 4915-59-7
• Molecular Formula: C11H11NO5
• Molecular Weight: 237.212
• Mol file: 4915-59-7.mol

Synonyms:

Chemical Property of N-benzoylaspartic acid

Chemical Property:

• Vapor Pressure: 6.76E-11mmHg at 25°C
• Boiling Point: 502°Cat760mmHg
• Flash Point: 257.4°C
• Density: 1.404g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-benzoylaspartic acid

There total 6 articles about N-benzoylaspartic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzoylaspartic acid (17966-68-6) → L-Aspartic acid (56-84-8,25608-40-6,27881-03-4,32505-46-7,52526-39-3) + D-N-benzoylaspartic acid (4915-59-7) + benzoyl L-aspartic acid (4631-12-3)

Guidance literature:

With D-glucose; corn steep liquor; fungus Beauveria bassiana ATCC 7159; In ethanol; water; for 72h; Title compound not separated from byproducts; Enzymatic reaction;

DOI:10.1007/s007060070095

Reference yield:

benzoyl chloride (98-88-4) → D-N-benzoylaspartic acid (4915-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH / H₂O / 2 h / 20 °C

2: corn steep liquor; fungus Beauveria bassiana ATCC 7159; glucose / ethanol; H₂O / 72 h / Enzymatic reaction

With sodium hydroxide; D-glucose; corn steep liquor; fungus Beauveria bassiana ATCC 7159; In ethanol; water; 1: Acylation / 2: Hydrolysis;

DOI:10.1007/s007060070095

Reference yield:

→ D-N-benzoylaspartic acid (4915-59-7)

Guidance literature:

With potassium permanganate; sulfuric acid; water;

DOI:10.1002/hlca.19300130610

upstream raw materials:

N-benzoylaspartic acid

benzoyl chloride

Refernces