Technology Process of Acetohydroxamic acid, N-(p-(p-chlorophenoxy)phenyl)-O-beta-D-glucopyranosyl-, hydrate (2:1)
There total 5 articles about Acetohydroxamic acid, N-(p-(p-chlorophenoxy)phenyl)-O-beta-D-glucopyranosyl-, hydrate (2:1) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) aq. ammonium chloride, zinc 2.) sodium hydrogen carbonate / 1.) dioxane, 15 min 2.) ether, water, 1.5 h
2: 14 percent / silver(I) carbonate / benzene / 24 h / Ambient temperature
3: 63 percent / barium methoxide / methanol / 1.5 h
4: sodium hydrogen carbonate, 4 A molecular sieves, triethylamine / dioxane / 2 h
With
4 A molecular sieve; ammonium chloride; barium methoxide; sodium hydrogencarbonate; triethylamine; silver carbonate; zinc;
In
1,4-dioxane; methanol; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 14 percent / silver(I) carbonate / benzene / 24 h / Ambient temperature
2: 63 percent / barium methoxide / methanol / 1.5 h
3: sodium hydrogen carbonate, 4 A molecular sieves, triethylamine / dioxane / 2 h
With
4 A molecular sieve; barium methoxide; sodium hydrogencarbonate; triethylamine; silver carbonate;
In
1,4-dioxane; methanol; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 35 percent / 2,6-lutidinium perchlorate / various solvent(s) / 25 h / Heating
2: 63 percent / barium methoxide / methanol / 1.5 h
3: sodium hydrogen carbonate, 4 A molecular sieves, triethylamine / dioxane / 2 h
With
4 A molecular sieve; barium methoxide; sodium hydrogencarbonate; triethylamine;
2,6-lutidinium perchlorate;
In
1,4-dioxane; methanol;