Technology Process of 2,2-Bis(3-chloropropyl)-1,3-dioxolane
There total 1 articles about 2,2-Bis(3-chloropropyl)-1,3-dioxolane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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1 Mol 1,7-Dichlor-heptanon-(4), 1 Mol Aethylenglykol u. p-Toluolsulfonsaeure in sd. Bzl. (13,5 h); Entfernung des entstehenden W.;
DOI:10.1021/ja01500a063
- Guidance literature:
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With
tetra-(n-butyl)ammonium iodide; sodium carbonate;
In
tetrahydrofuran; acetonitrile;
Heating;
DOI:10.1016/j.tetlet.2013.02.050
- Guidance literature:
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Multi-step reaction with 2 steps
1: 74 percent / butyllithium / tetrahydrofuran; hexane / -25 degC 12 h, 20 degC 12 h
2: cc HCl, glyoxylic-acid hydrate / acetonitrile / Ambient temperature
With
hydrogenchloride; n-butyllithium; 2,2-dihydroxyacetic acid;
In
tetrahydrofuran; hexane; acetonitrile;
DOI:10.1016/0040-4020(82)85007-2