2,2'-[Methylenebis(thio)]bisacetic acid nickel(II) salt

Base Information

• Chemical Name: 2,2'-[Methylenebis(thio)]bisacetic acid nickel(II) salt
• CAS No.: 71215-73-1
• Molecular Formula: C5H6O4S2*Ni
• Molecular Weight: 252.93
• Mol file: 71215-73-1.mol

Synonyms:

Chemical Property of 2,2'-[Methylenebis(thio)]bisacetic acid nickel(II) salt

Chemical Property:

• PSA: 130.86000
• LogP: -2.08990

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-[Methylenebis(thio)]bisacetic acid nickel(II) salt

There total 1 articles about 2,2'-[Methylenebis(thio)]bisacetic acid nickel(II) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylenedithiodiacetic acid (2068-24-8) + nickel dichloride (83864-14-6) → Ni(2+)*CH2(SCH2COO)2(2-)=Ni(CH2(SCH2COO)2) (71215-73-1)

Guidance literature:

With NaOH; In ethanol; water; aq. soln. of metal chloride was added to alc. soln. of ligand in equimolar amt., few drops concd. NaOH was added, reflux for 7 h; cooled with ice-cold water, filtered, washed with water, alc. and ether, dried in vac. over CaCl2, elem. anal.;

upstream raw materials:

methylenedithiodiacetic acid

nickel dichloride

Refernces