2-[(4-methylphenyl)amino]-1,1,2-triphenylethanol

Base Information

• Chemical Name: 2-[(4-methylphenyl)amino]-1,1,2-triphenylethanol
• CAS No.: 5469-99-8
• Molecular Formula: C₂₇H₂₅NO
• Molecular Weight: 379.502
• Mol file: 5469-99-8.mol

Synonyms:

Chemical Property of 2-[(4-methylphenyl)amino]-1,1,2-triphenylethanol

Chemical Property:

• Vapor Pressure: 3.08E-13mmHg at 25°C
• Boiling Point: 556.9°C at 760 mmHg
• Flash Point: 113.6°C
• Density: 1.166g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[(4-methylphenyl)amino]-1,1,2-triphenylethanol

There total 4 articles about 2-[(4-methylphenyl)amino]-1,1,2-triphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,2-triphenyl-2-p-tolylimino-ethyl hydroperoxide (103210-96-4) → 1,1,2-triphenyl-2-p-toluidino-ethanol (5469-99-8)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1021/ja01579a058

Reference yield:

2,2-diphenyl-N-p-tolyl-acetimidoyl chloride (102311-01-3) → 1,1,2-triphenyl-2-p-toluidino-ethanol (5469-99-8)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine

3: platinum; ethyl acetate / Hydrogenation

4: platinum; acetic acid / Hydrogenation

With acetic acid; ethyl acetate; triethylamine; platinum;

DOI:10.1021/ja01579a058

Reference yield:

phenylmagnesium bromide → 1,1,2-triphenyl-2-p-toluidino-ethanol (5469-99-8)

Guidance literature:

Multi-step reaction with 3 steps

2: platinum; ethyl acetate / Hydrogenation

3: platinum; acetic acid / Hydrogenation

With acetic acid; ethyl acetate; platinum;

DOI:10.1021/ja01579a058

upstream raw materials:

1,1,2-triphenyl-2-p-tolylimino-ethyl hydroperoxide

1,1,2-triphenyl-2-p-tolylimino-ethanol

2,2-diphenyl-N-p-tolyl-acetimidoyl chloride