Technology Process of 1-Azidopyrene
There total 5 articles about 1-Azidopyrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1-aminopyrene;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 ℃;
Inert atmosphere;
With
sodium azide;
In
water;
at 0 ℃;
for 0.416667h;
Inert atmosphere;
DOI:10.1021/jo200231k
- Guidance literature:
-
With
sodium azide; copper(ll) sulfate pentahydrate;
In
methanol;
at 20 ℃;
for 3h;
DOI:10.1021/ja407410b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal; ammonium formate / methanol / 3 h / Inert atmosphere; Reflux
2: hydrogenchloride; sodium nitrite / water-d2 / 0 - 5 °C
With
hydrogenchloride; palladium on activated charcoal; ammonium formate; sodium nitrite;
In
methanol; water-d2;
DOI:10.1039/c2cc34008a
