2,3-diphenyl-1H-indene

Base Information

• Chemical Name: 2,3-diphenyl-1H-indene
• CAS No.: 5324-00-5
• Molecular Formula: C21H16
• Molecular Weight: 268.358
• Mol file: 5324-00-5.mol

Synonyms:

Chemical Property of 2,3-diphenyl-1H-indene

Chemical Property:

• Vapor Pressure: 6.14E-06mmHg at 25°C
• Boiling Point: 390°Cat760mmHg
• Flash Point: 184.2°C
• Density: 1.136g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-diphenyl-1H-indene

There total 88 articles about 2,3-diphenyl-1H-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,c-2-diphenylindan-r-1-ol → 2,3-diphenyl-1H-indene (5324-00-5)

Guidance literature:

molybdophosphoric acid; silica gel; In chloroform; for 0.25h; Heating;

Reference yield: 94.0%

diphenyl acetylene (501-65-5) + 2-(chloromethyl)phenylboronic acid (374551-13-0) → 2,3-diphenyl-1H-indene (5324-00-5)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium carbonate; In 1,3-dioxane; water; at 50 ℃; for 20h; Inert atmosphere;

DOI:10.1021/ol8006887

Reference yield: 88.0%

(E)-phenyl(2-styrylphenyl)methanol (1323308-07-1) → 2,3-diphenyl-1H-indene (5324-00-5)

Guidance literature:

With p-TsOH immobilized on silica; In toluene; at 80 ℃; for 18h;

DOI:10.1021/acs.joc.8b01921

upstream raw materials:

2,3-diphenyl-1H-inden-1-one

3-Bromo-1,2-diphenylinden

2,3,3-triphenyl-prop-2-en-1-ol

1-(diphenylmethylidene)-2-(1-phenylethylidene)hydrazine

Downstream raw materials:

1-benzylidene-2,3-diphenyl-1H-indene

1-Dimethylamino-2.2-bis-<2.3-diphenyl-indenyliden-(1)-methyl>-ethylen

1-<5-Dimethylamino-pentadien-(2.4)-yliden>-2.3-diphenyl-inden

1-Dimethylaminomethylen-2.3-diphenyl-inden

Refernces

• 1、 Jongcharoenkamol, Jira,Chuathong, Patsapon,Amako, Yuka,Kono, Masato,Poonswat, Kasam,Ruchirawat, Somsak,Ploypradith, Poonsakdi. "Selective Divergent Synthesis of Indanols, Indanones, and Indenes via Acid-Mediated Cyclization of (Z)- and (E)-(2-Stilbenyl)methanols and Its Application for the Synthesis of Paucifloral F Derivatives". . p. 13184 - 13210. Retrieved 2018/11/02.
• 2、 Feng, Jie,Lu, Guoping,Lv, Meifang,Cai, Chun. "Palladium-catalyzed annulation of alkynes with ortho -halide-containing benzyl alcohols in aqueous medium". . p. 10561 - 10567. Retrieved 2015/02/19.