1-Fluorononane

Base Information

• Chemical Name: 1-Fluorononane
• CAS No.: 463-18-3
• Molecular Formula: C9H19 F
• Molecular Weight: 146.248
• Hs Code.: 29033990
• European Community (EC) Number: 630-616-0
• DSSTox Substance ID: DTXSID90196789
• Nikkaji Number: J64.701B
• Wikidata: Q83069802
• Mol file: 463-18-3.mol

Synonyms:1-FLUORONONANE;463-18-3;n-Nonyl fluoride;Nonyl fluoride;Nonane, 1-fluoro-;BRN 1733620;SCHEMBL45326;C9H19F;DTXSID90196789;C9-H19-F;MFCD00000455;AKOS007930382;LS-96858;FT-0607786

Chemical Property of 1-Fluorononane

Chemical Property:

• Appearance/Colour: clear colorless liquid
• Vapor Pressure: 2.53mmHg at 25°C
• Melting Point: -40°C
• Refractive Index: 1.402-1.404
• Boiling Point: 164.9°Cat760mmHg
• Flash Point: 85.3°C
• PSA: 0.00000
• Density: 0.801g/cm³
• LogP: 3.70650
• Storage Temp.: Flammables area
• XLogP3: 5.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 7
• Exact Mass: 146.147078768
• Heavy Atom Count: 10
• Complexity: 52.7

Purity/Quality:

99% ^*data from raw suppliers

1-Fluorononane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,Xn
• Hazard Codes: Xi,Xn
• Statements: 36/37/38-10-20/21/22
• Safety Statements: 37/39-26-16-45-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCF

Technology Process of 1-Fluorononane

There total 11 articles about 1-Fluorononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-fluoro-2-methyl-N,N-diisopropyl-propenylamine (65785-54-8) → n-nonyl fluoride (463-18-3) + N,N-diisopropylisobutyramide (6282-98-0)

Guidance literature:

With nonyl alcohol; In dichloromethane; 1.) 0 deg C; 2.) rt., 3h;

DOI:10.1016/S0040-4039(00)99407-3

Reference yield: 93.0%

nonyl alcohol (143-08-8) → n-nonyl fluoride (463-18-3) + N,N-diisopropylisobutyramide (6282-98-0)

Guidance literature:

With 1-fluoro-2-methyl-N,N-diisopropyl-propenylamine; In dichloromethane; 1.) 0 deg C; 2.) rt.,3h;

DOI:10.1016/S0040-4039(00)99407-3

Reference yield: 78.0%

1-fluorononanyl trifluoromethanesulfonate → n-nonyl fluoride (463-18-3)

Guidance literature:

With tetra-n-butylammonium hydride; In dichloromethane; at 20 ℃; for 17h; Inert atmosphere;

DOI:10.1016/j.jfluchem.2015.01.013

upstream raw materials:

1-Chlorononane

1-Bromononane

1-decanoic acid

1-fluoro-2-methyl-N,N-diisopropyl-propenylamine

Downstream raw materials:

dimethyl(nonyl)(phenyl)silane

Tridecane

3-methyldodec-1-ene

3-methyldodecane

Refernces

• 1、 Guijarro, David,Martínez, Pedro,Yus, Miguel. "Reductive defluorination of fluoroalkanes". . p. 1237 - 1244. Retrieved 2007/10/03.
• 2、 Munyemana, Francois,Frisque-Hesbain, Anne-Marie,Devos, Alain,Ghosez, Leon. "SYNTHESIS OF ALKYL HALIDES UNDER NEUTRAL CONDITIONS". . p. 3077 - 3080. Retrieved 2007/10/02.