9,10-Anthracenedione, 1-hydroxy-4-(methylamino)-

Base Information

• Chemical Name: 9,10-Anthracenedione, 1-hydroxy-4-(methylamino)-
• CAS No.: 6373-16-6
• Molecular Formula: C15H11 N O3
• Molecular Weight: 253.257
• Hs Code.: 2922509090
• European Community (EC) Number: 228-913-1
• NSC Number: 128426
• UNII: 9JSO4A4Z5U
• DSSTox Substance ID: DTXSID2064286
• Nikkaji Number: J70.161K
• Wikidata: Q81991412
• Mol file: 6373-16-6.mol

Synonyms:6373-16-6;Serisol Brilliant Blue R;C.I. Disperse Blue 22;1-(Methylamino)-4-hydroxyanthraquinone;9,10-Anthracenedione, 1-hydroxy-4-(methylamino)-;1-Hydroxy-4-(methylamino)anthraquinone;1-hydroxy-4-(methylamino)anthracene-9,10-dione;Anthraquinone, 1-hydroxy-4-(methylamino)-;C.I. 60715;9JSO4A4Z5U;EINECS 228-913-1;NSC 128426;NSC-128426;DISPERSE BLUE 22;UNII-9JSO4A4Z5U;SCHEMBL8427136;1-Methylamino-4-oxyanthrachinon;DTXSID2064286;9, 1-hydroxy-4-(methylamino)-;NSC128426;AKOS003617822;C.I.60715;1-HYDROXY-4-(METHYLAMINO)-9,10-ANTHRACENEDIONE;1-HYDROXY-4-METHYLAMINO-ANTHRAQUINONE(DISPERSE BLUE 22 C.I. 60715)

Chemical Property of 9,10-Anthracenedione, 1-hydroxy-4-(methylamino)-

Chemical Property:

• Vapor Pressure: 1.22E-10mmHg at 25°C
• Melting Point: 163 °C
• Boiling Point: 500.5°C at 760 mmHg
• PKA: 8.52±0.20(Predicted)
• Flash Point: 256.5°C
• PSA: 66.40000
• Density: 1.431g/cm³
• LogP: 2.28230
• XLogP3: 4.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 253.07389321
• Heavy Atom Count: 19
• Complexity: 395

Purity/Quality:

99% ^*data from raw suppliers

1-AMINO-4-HYDROXYANTHRAQUINONE-N-METHYL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1=C2C(=C(C=C1)O)C(=O)C3=CC=CC=C3C2=O

Technology Process of 9,10-Anthracenedione, 1-hydroxy-4-(methylamino)-

There total 11 articles about 9,10-Anthracenedione, 1-hydroxy-4-(methylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

1-(methylamino)-4-nitroanthraquinone (73888-68-3) → 1-methylamino-4-hydroxyanthraquinone (6373-16-6)

Guidance literature:

In isopropyl alcohol; for 1.08333h; Irradiation;

Reference yield:

1-(methylamino)anthraquinone (82-38-2) → 1-methylamino-4-hydroxyanthraquinone (6373-16-6)

Guidance literature:

With sulfuric acid; at 30 - 35 ℃;

Reference yield:

1,4-dihydroxy-9,10-anthracenedione (81-64-1,103220-12-8) + methylamine (74-89-5) → 1-methylamino-4-hydroxyanthraquinone (6373-16-6)

Guidance literature:

With manganese(II) sulfate; sodium carbonate; weiteres Reagens: Aethanol;

upstream raw materials:

1-bromo-4-(methylamino)-9,10-anthracenedione

1-(methylamino)anthraquinone

4-hydroxy-1-aminoanthraquinone

1-methoxy-4-methylamino-anthraquinone

Refernces