3,3-bis(cyanomethyl)-oxetane

Base Information

• Chemical Name: 3,3-bis(cyanomethyl)-oxetane
• CAS No.: 22030-97-3
• Molecular Formula: C7H8N2O
• Molecular Weight: 136.1512
• Mol file: 22030-97-3.mol

Synonyms:3,3-bis-cyanomethyl-oxetane;3,3-Bis-cyanmethyl-oxetan;3,3-Oxetanediacetonitrile;

Chemical Property of 3,3-bis(cyanomethyl)-oxetane

Chemical Property:

• Melting Point: 76.5 °C(Solv: benzene (71-43-2))
• Boiling Point: 342.8°Cat760mmHg
• Flash Point: 154.1°C
• PSA: 56.81000
• Density: 1.112g/cm³
• LogP: 0.83036

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3-bis(cyanomethyl)-oxetane

There total 3 articles about 3,3-bis(cyanomethyl)-oxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid-(3-chloro-2,2-bis-chloromethyl-propyl ester) (13103-49-6) → 3,3-bis-cyanomethyl-oxetane (22030-97-3)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol. alkaline solution

2: ethanol

With ethanol; alkaline solution;

DOI:10.1021/jo01360a008

Reference yield:

3,3-bis(chloromethyl)oxetane (78-71-7,25323-58-4) + sodium cyanide (143-33-9,25596-52-5) → 3,3-bis-cyanomethyl-oxetane (22030-97-3)

Guidance literature:

With ethanol;

DOI:10.1021/jo01360a008

Reference yield:

3,3-bis(bromomethyl)oxetane (2402-83-7) + sodium cyanide (143-33-9,25596-52-5) → 3,3-bis-cyanomethyl-oxetane (22030-97-3)

Guidance literature:

With ethanol;

upstream raw materials:

3,3-bis(chloromethyl)oxetane

sodium cyanide

3,3-bis(bromomethyl)oxetane

acetic acid-(3-chloro-2,2-bis-chloromethyl-propyl ester)

Downstream raw materials:

3,3-bis-carboxymethyl-oxetane