Technology Process of Benz(l)aceanthrylene
There total 7 articles about Benz(l)aceanthrylene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
aluminum oxide;
In
benzene;
for 0.75h;
Heating;
DOI:10.1021/jo00158a012
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 84 percent / zink dust, iodine / benzene; diethyl ether / 2 h / Heating
2: 1.) p-TsOH, 2.) 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ) / 1.) benzene, reflux, 2h, 2.) reflux, 6h
3: 91 percent / KOH / H2O; methanol / 1 h / Heating
4: 84 percent / anhydrous HF / 15 h / Ambient temperature
5: NaBH4 / tetrahydrofuran; methanol
6: Al2O3 / benzene / 0.75 h / Heating
With
aluminum oxide; potassium hydroxide; sodium tetrahydroborate; hydrogen fluoride; iodine; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc;
In
tetrahydrofuran; methanol; diethyl ether; water; benzene;
DOI:10.1021/jo00158a012