3-Methyl-1,5-pentanediyl diacrylate

Base Information

• Chemical Name: 3-Methyl-1,5-pentanediyl diacrylate
• CAS No.: 64194-22-5
• Molecular Formula: C12H18 O4
• Molecular Weight: 226.273
• Hs Code.: 2916190090
• European Community (EC) Number: 264-727-7
• DSSTox Substance ID: DTXSID40108418
• Nikkaji Number: J310.075H
• Mol file: 64194-22-5.mol

Synonyms:64194-22-5;3-Methyl-1,5-pentanediyl diacrylate;(3-methyl-5-prop-2-enoyloxypentyl) prop-2-enoate;3-Methylpentane-1,5-diyl diacrylate;EINECS 264-727-7;2-Propenoic acid, 1,1'-(3-methyl-1,5-pentanediyl) ester;3-METHYL-5-(PROP-2-ENOYLOXY)PENTYL PROP-2-ENOATE;SCHEMBL9103359;DTXSID40108418;3-Methylpentane-1,5-diyldiacrylate;3-methyl-1,5-pentanediol diacrylate;MFCD28968982;AKOS025296138;AS-62112;D80963

Chemical Property of 3-Methyl-1,5-pentanediyl diacrylate

Chemical Property:

• Vapor Pressure: 0.00142mmHg at 25°C
• Boiling Point: 296.6°C at 760 mmHg
• Flash Point: 138.9°C
• PSA: 52.60000
• Density: 1.009g/cm³
• LogP: 1.86110
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: Chloroform (Slightly), Methanol (Slightly)
• Water Solubility.: 541mg/L at 20.28℃
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 10
• Exact Mass: 226.12050905
• Heavy Atom Count: 16
• Complexity: 232

Purity/Quality:

99.9% ^*data from raw suppliers

3-Methyl-1,5-pentanediolDiacrylate(~0.5%4-HydroxyAnisoleasastabilizer) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(CCOC(=O)C=C)CCOC(=O)C=C
• Uses: 3-Methyl-1,5-pentanediol Diacrylate is a useful chemical reagent.

Technology Process of 3-Methyl-1,5-pentanediyl diacrylate

There total 2 articles about 3-Methyl-1,5-pentanediyl diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3-methylpentane-1,5-diol (4457-71-0) + acryloyl chloride (814-68-6,25189-84-8) → 3-methyl-1,5-pentanediol diacrylate (64194-22-5)

Guidance literature:

With triethylamine; 2-hydroxyresorcinol; In benzene; at 50 ℃; for 0.5h;

Reference yield:

3-methylglutaric anhydride (4166-53-4) → 3-methyl-1,5-pentanediol diacrylate (64194-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / lithium aluminium hydride / diethyl ether; tetrahydrofuran / 6.5 h / Heating

2: 50 percent / triethylamine, pyrogallol / benzene / 0.5 h / 50 °C

With lithium aluminium tetrahydride; triethylamine; 2-hydroxyresorcinol; In tetrahydrofuran; diethyl ether; benzene;

Reference yield: 38.0%

1,2,3,4-tetrahydro-1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline hydrochloride (6429-04-5,66820-84-6) + 3-methyl-1,5-pentanediol diacrylate (64194-22-5) → 3-[1-(3,4-Dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-propionic acid 5-{3-[1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-propionyloxy}-3-methyl-pentyl ester; compound with oxalic acid (81165-48-2)

Guidance literature:

In benzene; for 48h; Heating;

upstream raw materials:

3-methylpentane-1,5-diol

acryloyl chloride

3-methylglutaric anhydride

Downstream raw materials:

3-[1-(3,4-Dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-propionic acid 5-{3-[1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-propionyloxy}-3-methyl-pentyl ester; compound with oxalic acid

C₅₄H₇₄N₂O₁₂⁽²⁺⁾*2CH₃O₃S^(1-)

Refernces