Phenyldiazonium hexafluorophosphate

Base Information

• Chemical Name: Phenyldiazonium hexafluorophosphate
• CAS No.: 369-58-4
• Molecular Formula: C6H5F6N2P
• Molecular Weight: 250.083
• European Community (EC) Number: 206-721-9
• DSSTox Substance ID: DTXSID8059899
• Mol file: 369-58-4.mol

Synonyms:Phenyldiazonium hexafluorophosphate;369-58-4;Benzenediazonium hexafluorophosphate;Benzenediazonium, hexafluorophosphate(1-);benzenediazonium;hexafluorophosphate;EINECS 206-721-9;Benzenediazonium, hexafluorophosphate(1-) (1:1);C6H5N2.F6P;DTXSID8059899;SCHEMBL20395693;C6-H5-N2.F6-P;benzenediazonium hexafluorophos-phate;benzenediazonium hexafluorophosphate(V);FT-0715896

Chemical Property of Phenyldiazonium hexafluorophosphate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 41.74000
• Density: g/cm³
• LogP: 5.55358
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 0
• Exact Mass: 250.00945414
• Heavy Atom Count: 15
• Complexity: 168

Purity/Quality:

98%min ^*data from raw suppliers

PHENYLDIAZONIUM HEXAFLUOROPHOSPHATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)[N+]#N.F[P-](F)(F)(F)(F)F

Technology Process of Phenyldiazonium hexafluorophosphate

There total 11 articles about Phenyldiazonium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexafluorophosphoric acid + benzene diazonium chloride (100-34-5) → benzenediazonium hexafluorophosphate (369-58-4)

Guidance literature:

In not given; react. of 65% HPF6 with C6H5N2Cl;;

Reference yield:

Nitrosobenzene (586-96-9) → benzenediazonium hexafluorophosphate (369-58-4)

Guidance literature:

With water;

DOI:10.1021/ja01196a011

Reference yield:

phenylmagnesium bromide → benzenediazonium hexafluorophosphate (369-58-4)

Guidance literature:

With diethyl ether; cadmium(II) bromide;

upstream raw materials:

phenylhydrazine hydrochloride

2C₁₂H₂₄O₆*C₆H₅N₂⁽¹⁺⁾*F₆P^(1-)

Nitrosobenzene

N-phenyl benzoyl amide

Downstream raw materials:

chlorobenzene

phenol

1-Phenyl-3-<2-(thiomorpholino)ethyl>traizene

3-furfuryl-1-phenyltriazene

Refernces

• 1、 Krane, Jostein,Skjetne, Tore. "STUDIES OF CROWN ETHER COMPLEXES; ARYLDIAZONIUM ION COMPLEXES". . p. 1775 - 1778. Retrieved 2007/10/02.