Technology Process of 1H-[1,3]Dioxolo[4,5-j]pyrrolo[3,2,1-de]- phenanthridine-1,2-diol,2,3,3a,4,5,7,12b,12coctahydro-,(1R,2S,3aS,12bR,12cS)-
There total 40 articles about 1H-[1,3]Dioxolo[4,5-j]pyrrolo[3,2,1-de]- phenanthridine-1,2-diol,2,3,3a,4,5,7,12b,12coctahydro-,(1R,2S,3aS,12bR,12cS)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum on activated charcoal;
In
acetic acid;
under 1471.02 Torr;
Ambient temperature;
DOI:10.1016/S0031-9422(00)80145-4
- Guidance literature:
-
With
palladium; acetic acid;
Hydrogenation;
-
-
2188-68-3
(1S,2S,12bS,12cS)-1,2-diol-2,4,5,7,12b,12c-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridine hydrochloride
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium hydroxide / water / 16 h / 20 °C
2: acetic acid; palladium on activated charcoal; hydrogen / 20 h / 20 °C
With
ammonium hydroxide; palladium on activated charcoal; hydrogen; acetic acid;
In
water;
DOI:10.1021/acs.orglett.8b02562