sodium (Z)-octadec-9-enyl sulphate

Base Information

• Chemical Name: sodium (Z)-octadec-9-enyl sulphate
• CAS No.: 1847-55-8
• Molecular Formula: C18H36 O4 S . Na
• Molecular Weight: 370.529
• Hs Code.: 2920909090
• Mol file: 1847-55-8.mol

Synonyms:9-Octadecen-1-ol,hydrogen sulfate sodium salt, (Z)- (8CI);9-Octadecen-1-ol, hydrogen sulfate,sodium salt, (9Z)- (9CI);Cyclanon O;Duponol LS Flakes;IN 438;Oleyl sodiumsulfate;Oleyl sulfate sodium salt;Quolac EX-OS;Sodium oleyl alcohol sulfate;Sodium oleyl sulfate;Sulfopon O 680;

Chemical Property of sodium (Z)-octadec-9-enyl sulphate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 74.81000
• Density: g/cm³
• LogP: 6.58150

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium (Z)-octadec-9-enyl sulphate

There total 2 articles about sodium (Z)-octadec-9-enyl sulphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl oleate (112-62-9) → sodium (Z)-9-octadecene-1-sulfate (1847-55-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / diethyl ether

2: 1) SO₃*Me₃N, 2) a) 3 M aq. NaOH, b) Biorad AG 50W-X₄ (Na(+) form) ion-exchange resin / 1) 125 deg C, 6 h, 2) a) to pH 10, b) MeOH, 25 deg C, 4 h

With sodium hydroxide; lithium aluminium tetrahydride; trimethyl-sulfo-ammonium betaine; Biorad AG 50W-X₄ (Na(+) form) ion-exchange resin; In diethyl ether;

DOI:10.1021/jo00061a044

Reference yield:

oleoyl alcohol (143-28-2,593-47-5,84286-21-5) → sodium (Z)-9-octadecene-1-sulfate (1847-55-8)

Guidance literature:

With sodium hydroxide; trimethyl-sulfo-ammonium betaine; Biorad AG 50W-X₄ (Na(+) form) ion-exchange resin; Yield given. Multistep reaction; 1) 125 deg C, 6 h, 2) a) to pH 10, b) MeOH, 25 deg C, 4 h;

DOI:10.1021/jo00061a044

upstream raw materials:

oleoyl alcohol

Methyl oleate

Refernces