(2-hydroxytrimethylene)bis[dodecyldimethylammonium] dichloride

Base Information

• Chemical Name: (2-hydroxytrimethylene)bis[dodecyldimethylammonium] dichloride
• CAS No.: 50744-87-1
• Molecular Formula: C31H68 N2 O . 2 Cl
• Molecular Weight: 555.8
• Hs Code.: 2923900090
• Mol file: 50744-87-1.mol

Synonyms:1,3-Propanediaminium,N,N'-didodecyl-2-hydroxy-N,N,N',N'-tetramethyl-, dichloride (9CI)

Chemical Property of (2-hydroxytrimethylene)bis[dodecyldimethylammonium] dichloride

Chemical Property:

• PSA: 20.23000
• LogP: 2.34990

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2-hydroxytrimethylene)bis[dodecyldimethylammonium] dichloride

There total 7 articles about (2-hydroxytrimethylene)bis[dodecyldimethylammonium] dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N,N-dimethylaminododecane (112-18-5,83855-86-1) + 1,3-Dichloro-2-propanol (96-23-1) → 1,3?bis(dodecyldimethylammonio)?2?hydroxypropane dichloride (50744-87-1)

Guidance literature:

at 70 ℃; for 8h; Temperature;

DOI:10.1016/j.molliq.2019.03.008

Reference yield: 93.0%

N,N-dimethylaminododecane (112-18-5,83855-86-1) + dodecyldimethyl ammonium chloride (2016-48-0) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 1,3?bis(dodecyldimethylammonio)?2?hydroxypropane dichloride (50744-87-1)

Guidance literature:

In ethanol; 1.) RT, 8 h, 2.) reflux, 8 h;

DOI:10.1007/BF02523450

Reference yield: 92.87%

N,N-dimethylaminododecane (112-18-5,83855-86-1) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 1,3?bis(dodecyldimethylammonio)?2?hydroxypropane dichloride (50744-87-1)

Guidance literature:

With dodecyldimethyl ammonium chloride; In ethanol; at 80 ℃; for 8h;

DOI:10.1055/s-2002-34876

upstream raw materials:

N,N-dimethylaminododecane

1,3-Dichloro-2-propanol

dodecyldimethyl ammonium chloride

epichlorohydrin

Refernces

• 1、 Tamaddon, Fatemeh,Tadayonfar, SeydEhsan. "Comparative screening of tetra-chlorometallate anions in novel magnetic metallogeminisurfactant catalysts for advanced synthesis of an anti-tumor benzothiazol-based aminophosphonate drug (ACBTAP)". . p. 51 - 57. Retrieved 2019.
• 2、 Tamaddon, Fatemeh,Tadayonfar, SeydEhsan. "A novel bi-functional surfactant-based paramagnetic deep-eutectic catalyst for improved benzoin condensation and multi-component synthesis of pyrrole derivatives". . p. 71 - 78. Retrieved 2019/02/19.