Technology Process of 9-Anthracenecarbonitrile
There total 76 articles about 9-Anthracenecarbonitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-methyl-N-phenylformamide;
With
pyrophosphoryl chloride;
at 0 ℃;
for 0.5h;
anthracene;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 10h;
With
ammonia; iodine;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
regioselective reaction;
DOI:10.1016/j.tet.2012.04.034
- Guidance literature:
-
With
HCl·DMPU; hydroxylamine hydrochloride;
In
acetonitrile;
at 60 ℃;
DOI:10.1039/d0gc00757a
- Guidance literature:
-
9-anthracenealdehyde oxime;
With
2-chloro-1-methyl-pyridinium iodide;
In
dichloromethane;
at 20 ℃;
for 0.166667h;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1081/SCC-120034158
Xn
