2-Ethyl-2-adamantyl methacrylate

Base Information

• Chemical Name: 2-Ethyl-2-adamantyl methacrylate
• CAS No.: 209982-56-9
• Deprecated CAS: 929020-23-5,1334478-15-7,1402927-36-9,1772655-42-1,2055849-97-1
• Molecular Formula: C16H24O2
• Molecular Weight: 248.365
• Hs Code.: 2933998090
• European Community (EC) Number: 805-827-8
• DSSTox Substance ID: DTXSID60943303
• Nikkaji Number: J1.334.591K
• Wikidata: Q72472240
• Mol file: 209982-56-9.mol

Synonyms:209982-56-9;2-ETHYL-2-ADAMANTYL METHACRYLATE;(2-ethyl-2-adamantyl) 2-methylprop-2-enoate;2-Propenoic acid, 2-methyl-, 2-ethyltricyclo[3.3.1.13,7]dec-2-yl ester;2-ethyladamantan-2-yl methacrylate;Methacrylic Acid 2-Ethyl-2-adamantyl Ester;2-ethyladamantan-2-yl 2-methylprop-2-enoate;2-Ethyl-2-methacryloyloxyadamantane (stabilized with MEHQ);2-Ethyl-2-methacryloyloxyadamantane;2-Propenoic acid, 2-methyl-, 2-ethyltricyclo(3.3.1.13,7)dec-2-yl ester;SCHEMBL44041;SCHEMBL14445711;SCHEMBL15166571;SCHEMBL23254207;2-Ethyl-2-adamanthylmethacrylate;2-ethyladamantan-2-ylmethacrylate;DTXSID60943303;DCTVCFJTKSQXED-UHFFFAOYSA-N;AMY11176;BCP25688;MFCD06411144;AKOS015918096;AC-32093;AS-72662;E0909;FT-0717669;T72066;2-Ethacryloyloxy-2-methyladamantane;2-Ethyladamant-2-yl methacrylate;(1R,3R,5R,7R)-2-ETHYLADAMANTAN-2-YL 2-METHYLPROP-2-ENOATE

Chemical Property of 2-Ethyl-2-adamantyl methacrylate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 40 °C
• Refractive Index: 1.513
• Boiling Point: 318.253 °C at 760 mmHg
• Flash Point: 130.896 °C
• PSA: 26.30000
• Density: 1.047 g/cm³
• LogP: 3.71060
• Storage Temp.: <0°C
• Solubility.: soluble in Methanol
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 248.177630004
• Heavy Atom Count: 18
• Complexity: 355

Purity/Quality:

99%min ^*data from raw suppliers

2-Ethyl-2-methacryloyloxyadamantane (stabilized with MEHQ) >97.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1(C2CC3CC(C2)CC1C3)OC(=O)C(=C)C

Technology Process of 2-Ethyl-2-adamantyl methacrylate

There total 1 articles about 2-Ethyl-2-adamantyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Adamantanone (700-58-3) + adamantane (281-23-2) + 2-ethyl-2-adamantanol (14648-57-8) → 2-ethyladamantan-2-yl methacrylate (209982-56-9) + N,N,N',N'-tetraethylurea (1187-03-7)

Guidance literature:

Reference yield:

2-ethyladamantan-2-yl methacrylate (209982-56-9) → C29H39F2O10S(1-)*C18H15S(1+)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / chloroform / 18 h / 23 °C

2.1: acetonitrile / 2 h / 23 °C

3.1: sodium tetrahydroborate / acetonitrile; water / 18.5 h / 5 - 23 °C

4.1: chloroform / 1 h / 23 - 60 °C

4.2: 2 h / 23 °C

With sodium tetrahydroborate; osmium(VIII) oxide; 4-methylmorpholine N-oxide; In chloroform; water; acetonitrile;

upstream raw materials:

2-Adamantanone

adamantane

2-ethyl-2-adamantanol

Refernces