1-Chloro-2-nitroethane

Base Information

• Chemical Name: 1-Chloro-2-nitroethane
• CAS No.: 625-47-8
• Molecular Formula: C2H4ClNO2
• Molecular Weight: 109.512
• Hs Code.: 2904909090
• Mol file: 625-47-8.mol

Synonyms:2-Chloronitroethane;Ethane, 1-chloro-2-nitro-;1-Chlor-2-nitroaethan;1-chloro-2-nitro-ethane;1-Chlor-2-nitro-ethan;Ethane,1-chloro-2-nitro;

Chemical Property of 1-Chloro-2-nitroethane

Chemical Property:

• Vapor Pressure: 1.26mmHg at 25°C
• Refractive Index: 1.4070 (estimate)
• Boiling Point: 173.5°Cat760mmHg
• Flash Point: 56.5°C
• PSA: 45.82000
• Density: 1.277g/cm³
• LogP: 1.02510

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Chloro-2-nitroethane

There total 2 articles about 1-Chloro-2-nitroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethene (74-85-1) + dichloromethane (75-09-2) → 1-chloro-2-nitroethane (625-47-8) + 2-chloro-ethanol (107-07-3)

Guidance literature:

at -5 - 0 ℃; und anschliessenden Behandeln mit Methanol;

DOI:10.1039/jr9580001955

Reference yield:

Nitroethane (79-24-3) → 1-chloro-1-nitroethane (598-92-5) + 1-chloro-2-nitroethane (625-47-8)

Guidance literature:

With Oxone; sodium chloride; In chloroform; water; at 20 ℃; for 4h; Overall yield = 97 %Spectr.; Sealed tube; Irradiation;

DOI:10.1021/acs.orglett.7b02153

Reference yield: 76.0%

1-chloro-2-nitroethane (625-47-8) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → 5-Nitrobicyclo<2.2.1>hept-2-en (768-16-1)

Guidance literature:

With N,N-bis(trimethylsilyl)acetamide; -15 deg C, 1 h; -15 deg C to 20 deg C;

upstream raw materials:

ethene

dichloromethane

Nitroethane

Downstream raw materials:

2-nitro-1-ethanol

1-nitroethylene

1-nitro-2-phenylaminoethane

N-(4-chloro-3-sulfamoylphenyl)-2-nitroethyleneamine

Refernces