Piperazine, 1,4-dimethyl-, 1,4-dioxide (9CI)

Base Information

• Chemical Name: Piperazine, 1,4-dimethyl-, 1,4-dioxide (9CI)
• CAS No.: 35190-65-9
• Molecular Formula: C₆H₁₄N₂O₂
• Molecular Weight: 146.189
• Mol file: 35190-65-9.mol

Synonyms:N,N-Dimethylpiperazinedioxide; N,N'-Dimethyldioxidopiperazine; NSC 367800

Chemical Property of Piperazine, 1,4-dimethyl-, 1,4-dioxide (9CI)

Chemical Property:

• Melting Point: 283-284℃
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 58.86000
• Density: g/cm³
• LogP: -0.19360

Purity/Quality:

99% ^*data from raw suppliers

N,N-DIMETHYLPIPERAZINEDIOXIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Piperazine, 1,4-dimethyl-, 1,4-dioxide (9CI)

There total 5 articles about Piperazine, 1,4-dimethyl-, 1,4-dioxide (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-dimethylpiperazine (106-58-1) → trans-1,4-dimethylpiperazine 1,4-dioxide (35190-65-9) + 1,4-Dimethyl-piperazine 1,4-dioxide (35190-65-9)

Guidance literature:

With dihydrogen peroxide; In acetone; at 100 ℃; Yield given. Yields of byproduct given;

DOI:10.1021/jo00323a035

Reference yield:

N,N'-dimethylpiperazine (106-58-1) → trans-1,4-dimethylpiperazine 1,4-dioxide (35190-65-9) + 1,4-Dimethyl-piperazine 1,4-dioxide (35190-65-9)

Guidance literature:

With dihydrogen peroxide; In acetone; at 100 ℃; Yield given. Yields of byproduct given;

DOI:10.1021/jo00323a035

Reference yield:

C20H24N2O4(2+)*2FO3S(1-) → trans-1,4-dimethylpiperazine 1,4-dioxide (35190-65-9) + 1,4-Dimethyl-piperazine 1,4-dioxide (35190-65-9)

Guidance literature:

In water; for 15h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/jo00323a035

upstream raw materials:

N,N'-dimethylpiperazine

Refernces