3-Bromophenylhydrazine

Base Information

• Chemical Name: 3-Bromophenylhydrazine
• CAS No.: 40887-80-7
• Molecular Formula: C6H7BrN2
• Molecular Weight: 187.039
• Hs Code.: 2928000090
• European Community (EC) Number: 255-130-2
• DSSTox Substance ID: DTXSID20193862
• Nikkaji Number: J294.781A
• Wikidata: Q83066585
• Mol file: 40887-80-7.mol

Synonyms:(3-bromophenyl)hydrazine;3-Bromophenylhydrazine;40887-80-7;Hydrazine, (3-bromophenyl)-;(3-Bromo-phenyl)-hydrazine;EINECS 255-130-2;3-bromo-phenylhydrazine;3-bromophenyl hydrazine;3-Bromo-phenyl-hydrazine;SCHEMBL7658;1-(3-Bromophenyl)hydrazine;1-(3-Bromophenyl)hydrazine #;DTXSID20193862;BBL020531;MFCD02656654;STK893220;AKOS002680087;AB11945;AM86953;FS-5147;BB 0249785;CS-0452351;F81450

Chemical Property of 3-Bromophenylhydrazine

Chemical Property:

• Boiling Point: 174-176 °C(Press: 20 Torr)
• PKA: 4.91±0.10(Predicted)
• PSA: 38.05000
• Density: 1.666±0.06 g/cm3(Predicted)
• LogP: 2.50800
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 185.97926
• Heavy Atom Count: 9
• Complexity: 87.1

Purity/Quality:

98%min ^*data from raw suppliers

(3-bromophenyl)hydrazine ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)Br)NN

Technology Process of 3-Bromophenylhydrazine

There total 4 articles about 3-Bromophenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-Bromoaniline (591-19-5) → 3-bromophenylhydrazine (40887-80-7)

Guidance literature:

With hydrogenchloride; tin(ll) chloride; sodium nitrite; Diazotization;

Reference yield:

3-bromophenylhydrazine hydrochloride (27246-81-7) → 3-bromophenylhydrazine (40887-80-7)

Guidance literature:

With water; In ethanol; water;

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + 3-bromophenyldiazonium chloride (20893-74-7) → 3-bromophenylhydrazine (40887-80-7)

Guidance literature:

upstream raw materials:

m-Bromoaniline

hydrogenchloride

3-bromophenyldiazonium chloride

3-bromophenylhydrazine hydrochloride

Downstream raw materials:

5-bromo-1,2,3,4-tetrahydrocarbazole

7-bromo-2,3,4,9-tetrahydro-1H-carbazole

5-amino-1-(3-bromophenyl)-1H-pyrazole-4-carbonitrile

ethyl 1-(3-bromophenyl)-3-methyl-pyrazol-5-yl carboxylate

Refernces

• 1、 -. "HUMAN PLASMA KALLIKREIN INHIBITORS". Page/Page column 139; 140. . Retrieved 2015/11/02.
• 2、 -. "CARBOLINE CARBOXAMIDE COMPOUNDS USEFUL AS KINASE INHIBITORS". Page/Page column 180-182. . Retrieved 2012/01/06.