1-(2-Bromoethoxy)-4-methoxybenzene

Base Information

• Chemical Name: 1-(2-Bromoethoxy)-4-methoxybenzene
• CAS No.: 22921-76-2
• Molecular Formula: C9H11BrO2
• Molecular Weight: 231.089
• Hs Code.: 2909309090
• Mol file: 22921-76-2.mol

Synonyms:1-(2-Bromoethoxy)-4-methoxybenzene;4-(2-Bromoethoxy)anisole;4-(2-Bromoethoxy)-1-methoxybenzene;

Chemical Property of 1-(2-Bromoethoxy)-4-methoxybenzene

Chemical Property:

• Appearance/Colour: Off-white to pink-beige crystalline powder
• Vapor Pressure: 0.00335mmHg at 25°C
• Melting Point: 46-50 °C
• Refractive Index: 1.534
• Boiling Point: 291.7 °C at 760 mmHg
• Flash Point: 129.6 °C
• PSA: 18.46000
• Density: 1.382 g/cm³
• LogP: 2.46890

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-(2-Bromoethoxy)-4-methoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37/39-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-Bromoethoxy)-4-methoxybenzene

There total 5 articles about 1-(2-Bromoethoxy)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-(4-methoxyphenoxy)ethanol (5394-57-0) → 1-(2-bromoethoxy)-4-methoxybenzene (22921-76-2)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In acetonitrile;

DOI:10.1039/c3ra41345d

Reference yield: 70.0%

4-methoxy-phenol (150-76-5) + ethylene dibromide (106-93-4) → 1-(2-bromoethoxy)-4-methoxybenzene (22921-76-2)

Guidance literature:

With sodium hydroxide; for 5h; Heating;

Reference yield:

4-methoxy-phenol (150-76-5) → 1-(2-bromoethoxy)-4-methoxybenzene (22921-76-2)

Guidance literature:

upstream raw materials:

4-methoxy-phenol

ethylene dibromide

potassium p-methoxyphenolate

2-(4-methoxyphenoxy)ethanol

Downstream raw materials:

2-[2-(4-methoxy-phenoxy)-ethylamino]-ethanol

1,1-difluoro-4-(4'-methoxyphenoxy)propyl phenyl sulfide

C₁₃H₁₇N₂O₂⁽¹⁺⁾*Br^(1-)

C₁₃H₁₇N₂O₂⁽¹⁺⁾*C₂F₆NO₄S₂^(1-)

Refernces

• 1、 Gouda, Chinmayananda,Barik, Debashis,Maitra, Chandrima,Liang, Kai-Chieh,Ho, Feng-Cheng,Srinivasadesikan, Venkatesan,Chandran, Sarala,Wu, Shu-Pao,Lin, Ming-Chang,Lin, Hong-Cheu. "Application of stimuli-responsive FRET behavior toward cyanide detection in a photo-switchable [2]pseudorotaxane polymer containing the BODIPY donor and the merocyanine acceptor". supporting information. p. 2321 - 2333. Retrieved 2021/03/06.
• 2、 -. "1-aryloxy ethyl piperidine-4-yl benzophenone derivative as well as preparation method and application thereof". Paragraph 0040-0042. . Retrieved 2019/11/20.