(2Z)-3-(3,4-dimethylphenyl)-2-[(3,4-dimethylphenyl)imino]-5-[(4-hydroxy-3,5-dimethoxyphenyl)methylidene]-1,3-thiazolidin-4-one

Base Information

• Chemical Name: (2Z)-3-(3,4-dimethylphenyl)-2-[(3,4-dimethylphenyl)imino]-5-[(4-hydroxy-3,5-dimethoxyphenyl)methylidene]-1,3-thiazolidin-4-one
• CAS No.: 6453-93-6
• Molecular Formula: C21H14 O
• Molecular Weight: 282.342
• Mol file: 6453-93-6.mol

Synonyms:Ketone,1-phenanthryl phenyl (6CI,7CI,8CI); 1-Benzoylphenanthrene; NSC 408010

Chemical Property of (2Z)-3-(3,4-dimethylphenyl)-2-[(3,4-dimethylphenyl)imino]-5-[(4-hydroxy-3,5-dimethoxyphenyl)methylidene]-1,3-thiazolidin-4-one

Chemical Property:

• Vapor Pressure: 2.14E-19mmHg at 25°C
• Boiling Point: 685.1°C at 760 mmHg
• Flash Point: 368.1°C
• Density: 1.21g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2Z)-3-(3,4-dimethylphenyl)-2-[(3,4-dimethylphenyl)imino]-5-[(4-hydroxy-3,5-dimethoxyphenyl)methylidene]-1,3-thiazolidin-4-one

There total 4 articles about (2Z)-3-(3,4-dimethylphenyl)-2-[(3,4-dimethylphenyl)imino]-5-[(4-hydroxy-3,5-dimethoxyphenyl)methylidene]-1,3-thiazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylmagnesium bromide → 1-benzoylphenanthrene (6453-93-6)

Guidance literature:

With diethyl ether; benzene; Erwaermen auf Siedetemperatur; Hydrolyse des erhaltenen Phenyl--keton-imins;

DOI:10.1021/ja01306a051

Reference yield:

phenanthrene (85-01-8) + benzoyl chloride (98-88-4) → 1-benzoylphenanthrene (6453-93-6)

Guidance literature:

With carbon disulfide; aluminium trichloride;

DOI:10.1021/jo01227a009 DOI:10.1021/ja01306a051

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + aluminium trichloride (7446-70-0) + phenanthrene (85-01-8) + benzoyl chloride (98-88-4) → phenanthrene-9-yl (phenyl)methanone (6453-95-8) + 1-benzoylphenanthrene (6453-93-6)

Guidance literature:

DOI:10.1021/jo01227a009 DOI:10.1021/ja01306a051

upstream raw materials:

carbon disulfide

aluminium trichloride

phenanthrene

benzoyl chloride

Downstream raw materials:

benzoic acid

1-(1-phenanthryl)-1-phenyl-2-methyl-1-propene

1-benzoyl-9,10-epoxy-9,10-dihydrophenanthrene

phenanthrene-1-carbanilide