2,2-dimethylthietane

Base Information

• Chemical Name: 2,2-dimethylthietane
• CAS No.: 55022-72-5
• Molecular Formula: C5H10S
• Molecular Weight: 102.1979
• Mol file: 55022-72-5.mol

Synonyms:

Chemical Property of 2,2-dimethylthietane

Chemical Property:

• Vapor Pressure: 25.6mmHg at 25°C
• Boiling Point: 112.5°C at 760 mmHg
• Flash Point: 14.5°C
• Density: 0.938g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2-dimethylthietane

There total 3 articles about 2,2-dimethylthietane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Methyl-3-sulfanylbutan-1-ol (34300-94-2) → 2,2-Dimethylthietane (55022-72-5)

Guidance literature:

With diethoxyltriphenylphosphorane; In toluene; at -25 ℃; for 6h; Yield given;

Reference yield:

3-Methyl-3-sulfanylbutan-1-ol (34300-94-2) + diethoxyltriphenylphosphorane (86852-11-1,18509-25-6) → 2,2-Dimethylthietane (55022-72-5) + 4-ethylthio-4-methylbutanol

Guidance literature:

In toluene; at 25 ℃;

Reference yield:

→ 2,2-Dimethylthietane (55022-72-5)

Guidance literature:

aus /BRN= 605330/ in mehreren Stufen;

upstream raw materials:

3-Methyl-3-sulfanylbutan-1-ol

diethoxyltriphenylphosphorane

Refernces

• 1、 Robinson, Philip L.,Kelly, Jeffery W.,Slayton, A. Evans. "THE CHEMISTRY OF α,ω-MERCAPTOALCOHOLS IN THE PRESENCE OF DIETHOXYTRIPHENYLPHOSPHORANE. TEMEPERATURE DEPENDENCE OF CYCLODEHYDRATIONS AND S-ETHYLATIONS". . p. 59 - 70. Retrieved 2007/10/02.