MOP

Base Information

• Chemical Name: MOP
• CAS No.: 34374-04-4
• Molecular Formula: C25H38O2
• Molecular Weight: 370.57
• Hs Code.: 2906299090
• Mol file: 34374-04-4.mol

Synonyms:6,6,9-trimethyl-3-(1-methyl-octyl)-7,8,9,10-tetrahydro-6H-benzo[c]chromen-1-ol;Methyloctylpyran;3-Methyloctyl-7,8,9,10-tetrahydrocannabinol;6H-Dibenzo(b,d)pyran-1-ol,3-(1'-methyloctyl)-7,8,9,10-tetrahydro-6,6,9-trimethyl;

Chemical Property of MOP

Chemical Property:

• Vapor Pressure: 4.48E-10mmHg at 25°C
• Boiling Point: 486.1°C at 760 mmHg
• PKA: 10.03±0.60(Predicted)
• Flash Point: 199.5°C
• PSA: 29.46000
• Density: 1.03g/cm³
• LogP: 7.60080
• Storage Temp.: -20°C

Purity/Quality:

99%, ^*data from raw suppliers

OPN4 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of MOP

There total 2 articles about MOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-methyl-2-cyclohexanone-1-carboxylate (13537-82-1) → 6,6,9-trimethyl-3-(1-methyl-octyl)-7,8,9,10-tetrahydro-6H-benzo[c]chromen-1-ol (34374-04-4)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphoryl chloride; benzene

2: diethyl ether; benzene

With diethyl ether; trichlorophosphate; benzene;

DOI:10.1021/ja01182a067

Reference yield:

methyl magnesium iodide (917-64-6) + 1-hydroxy-9-methyl-3-(1-methyl-octyl)-7,8,9,10-tetrahydro-benzo[c]chromen-6-one → 6,6,9-trimethyl-3-(1-methyl-octyl)-7,8,9,10-tetrahydro-6H-benzo[c]chromen-1-ol (34374-04-4)

Guidance literature:

With diethyl ether; benzene;

DOI:10.1021/ja01182a067

upstream raw materials:

methyl magnesium iodide

ethyl 4-methyl-2-cyclohexanone-1-carboxylate