Technology Process of 9-Oxa-10-selenaanthracene
There total 12 articles about 9-Oxa-10-selenaanthracene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
selenium; trimethylsilyl cyanide;
In
dimethyl sulfoxide;
at 140 ℃;
for 24h;
Schlenk technique;
Green chemistry;
DOI:10.1002/chem.202004005
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique
1.2: -78 - 20 °C / Inert atmosphere; Schlenk technique
2.1: silver(I) nitrite; selenium; dipotassium peroxodisulfate / 1,4-dioxane / 24 h / 130 °C / Schlenk technique
With
selenium; dipotassium peroxodisulfate; silver(I) nitrite; n-butyllithium;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/adsc.202001006
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) iodide; potassium phosphate; dimethylaminoacetic acid / 50 °C / Inert atmosphere; Schlenk technique
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere; Schlenk technique
2.2: -78 - 20 °C / Inert atmosphere; Schlenk technique
3.1: silver(I) nitrite; selenium; dipotassium peroxodisulfate / 1,4-dioxane / 24 h / 130 °C / Schlenk technique
With
selenium; potassium phosphate; dipotassium peroxodisulfate; copper(l) iodide; silver(I) nitrite; n-butyllithium; dimethylaminoacetic acid;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/adsc.202001006
