4,4,4-TRIFLUOROBUTYLAMINE HYDROCHLORIDE 97

Base Information

• Chemical Name: 4,4,4-TRIFLUOROBUTYLAMINE HYDROCHLORIDE 97
• CAS No.: 84153-82-2
• Molecular Formula: C4H9ClF3N
• Molecular Weight: 163.57
• Hs Code.: 2921199090
• Mol file: 84153-82-2.mol

Synonyms:1-Butanamine,4,4,4-trifluoro-, hydrochloride (9CI);(4,4,4-Trifluorobutyl)aminehydrochloride;4,4,4-trifluorobutan-1-amine hydrochloride (1:1);1-butanamine, 4,4,4-trifluoro-, hydrochloride (1:1);

Chemical Property of 4,4,4-TRIFLUOROBUTYLAMINE HYDROCHLORIDE 97

Chemical Property:

• Vapor Pressure: 148mmHg at 25°C
• Melting Point: 130-131 °C(Solv: ethyl acetate (141-78-6))
• Boiling Point: 67.1 °C at 760 mmHg
• Flash Point: 3.6 °C
• PSA: 26.02000
• LogP: 2.78990
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

4,4,4-Trifluorobutan-1-amineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4,4-TRIFLUOROBUTYLAMINE HYDROCHLORIDE 97

There total 3 articles about 4,4,4-TRIFLUOROBUTYLAMINE HYDROCHLORIDE 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4,4-trifluorobutanol (461-18-7) → 4,4,4-trifluorobutan-1-amine hydrochloride (84153-82-2)

Guidance literature:

4,4,4-trifluorobutanol; With iminodicarboxylic acid di-tert-butyl ester; triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 - 25 ℃; for 18h;

With trifluoroacetic acid; at 0 - 20 ℃; for 24h;

Reference yield:

C14H24F3NO4 → 4,4,4-trifluorobutan-1-amine hydrochloride (84153-82-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 0 - 15 ℃; for 12h;

Reference yield:

4,4,4-trifluorobutan-1-amine (819-46-5) → 4,4,4-trifluorobutan-1-amine hydrochloride (84153-82-2)

Guidance literature:

With hydrogenchloride; In diethyl ether;

upstream raw materials:

4,4,4-trifluorobutan-1-amine

4,4,4-trifluorobutanol

Downstream raw materials:

4,4,4-trifluorobutanol

4,4,4-trifluoro-2-butanol

Refernces

• 1、 -. "NEW COMPOUNDS I/418". Page/Page column 30. . Retrieved 2008/06/13.