Technology Process of 7-(Diphenylmethylene)bicyclo(2.2.1)heptan-2-ol
There total 7 articles about 7-(Diphenylmethylene)bicyclo(2.2.1)heptan-2-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 15h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 82 percent / sodium ethoxide / ethanol / 3.5 h
2: benzene / 1848 h / 40 °C
3: 5percent Pd/C, H2 / ethyl acetate / 760 Torr
4: 86 percent / aq. potassium hydroxide / dimethylsulfoxide / 13 h
5: BMS
With
potassium hydroxide; palladium on activated charcoal; dimethylsulfide borane complex; hydrogen; sodium ethanolate;
In
ethanol; dimethyl sulfoxide; ethyl acetate; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 1848 h / 40 °C
2: 5percent Pd/C, H2 / ethyl acetate / 760 Torr
3: 86 percent / aq. potassium hydroxide / dimethylsulfoxide / 13 h
4: BMS
With
potassium hydroxide; palladium on activated charcoal; dimethylsulfide borane complex; hydrogen;
In
dimethyl sulfoxide; ethyl acetate; benzene;