Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]-

Base Information

• Chemical Name: Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]-
• CAS No.: 41642-51-7
• Deprecated CAS: 54077-21-3,81232-37-3,81232-37-3
• Molecular Formula: C20H19N7O3
• Molecular Weight: 405.416
• Hs Code.: 2927000090
• European Community (EC) Number: 255-473-8
• DSSTox Substance ID: DTXSID8068335
• Nikkaji Number: J30.099C
• Mol file: 41642-51-7.mol

Synonyms:41642-51-7;DISPERSE BLUE 165;N-(2-((2,6-Dicyano-4-nitrophenyl)diazenyl)-5-(diethylamino)phenyl)acetamide;Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]-;EINECS 255-473-8;C.I.Disperse Blue 165;C.I. Disperse Blue 165;C20H19N7O3;N-[2-[(2,6-dicyano-4-nitrophenyl)diazenyl]-5-(diethylamino)phenyl]acetamide;N-(2-((2,6-Dicyano-4-nitrophenyl)azo)-5-(diethylamino)phenyl)acetamide;N-2-(2,6-Dicyano-4-nitrophenyl)azo-5-(diethylamino)phenylacetamide;Acetamide, N-(2-((2,6-dicyano-4-nitrophenyl)azo)-5-(diethylamino)phenyl)-;N-(2-((4-Nitro-2,6-dicyanophenyl)azo)-5-(diethylamino)phenyl)acetamide;N-[2-[(2,6-Dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]acetamide;Acetamide, N-(2-(2-(2,6-dicyano-4-nitrophenyl)diazenyl)-5-(diethylamino)phenyl)-;Disperse Blue BBLS;DTXSID8068335;SCHEMBL11222989;MFCD00468019;AKOS016009339;C20-H19-N7-O3;W-110958;Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl) azo]-5-(diethylamino)phenyl]-

Chemical Property of Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]-

Chemical Property:

• Appearance/Colour: dark blue powder
• Vapor Pressure: 5.94E-19mmHg at 25°C
• Refractive Index: 1.631
• Boiling Point: 691.2 °C at 760 mmHg
• PKA: 14.02±0.70(Predicted)
• Flash Point: 371.8 °C
• PSA: 150.46000
• Density: 1.28 g/cm³
• LogP: 5.15436
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 6
• Exact Mass: 405.15493749
• Heavy Atom Count: 30
• Complexity: 717

Purity/Quality:

99.9% ^*data from raw suppliers

Disperse Blue 165 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC(=C(C=C1)N=NC2=C(C=C(C=C2C#N)[N+](=O)[O-])C#N)NC(=O)C

Technology Process of Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]-

There total 14 articles about Acetamide, N-[2-[(2,6-dicyano-4-nitrophenyl)azo]-5-(diethylamino)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.5%

→ D7 (41642-51-7)

Guidance literature:

Reference yield: 60.0%

1-amino-2,6-dicyano-4-nitrobenzene (20033-48-1) + m-acetylamino-N,N-diethylanilne (6375-46-8) → D7 (41642-51-7)

Guidance literature:

With phosphoric acid; sulfuric acid; sodium nitrite; at 0 ℃; for 4h;

Reference yield:

copper(I) cyanide (544-92-3) + N-[2-(2,6-Dibromo-4-nitro-phenylazo)-5-diethylamino-phenyl]-acetamide (52583-53-6) → D7 (41642-51-7)

Guidance literature:

With dicyanozinc; In N,N-dimethyl-formamide; at 110 ℃; for 3h; Yield given;

upstream raw materials:

copper(I) cyanide

N-[2-(2,6-Dibromo-4-nitro-phenylazo)-5-diethylamino-phenyl]-acetamide

1-amino-2,6-dicyano-4-nitrobenzene

m-acetylamino-N,N-diethylanilne

Refernces

• 1、 Thiel, W.,Mayer, R.,Jauer, E.-A.,Modrow, H.,Dost, H.. "Synthesis and Spectral Characterization of Blue Dyes of the Benzene Series". . p. 497 - 514. Retrieved 2007/10/02.
• 2、 -. "Process for the preparation of cyano azo dyestuffs". . . Retrieved 2008/06/13.