Praseodymium antimonide

Base Information

• Chemical Name: Praseodymium antimonide
• CAS No.: 12066-81-8
• Molecular Formula: PrSb
• Molecular Weight: 262.658
• European Community (EC) Number: 235-071-9
• Mol file: 12066-81-8.mol

Synonyms:Praseodymium antimonide;antimony;praseodymium(3+);EINECS 235-071-9;12066-81-8;Antimony, compound with praseodymium (1:1);Pr.Sb;Praseodymium antimonide (PrSb)

Chemical Property of Praseodymium antimonide

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 261.81147
• Heavy Atom Count: 2
• Complexity: 0

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [Sb].[Pr+3]

Technology Process of Praseodymium antimonide

There total 4 articles about Praseodymium antimonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

praseodymium + antimony (7440-36-0) → praseodymium monoantimonide (12066-81-8)

Guidance literature:

A mixture of the elements was induction molten in a small Ta crucible (sealed by welding under argon).;

DOI:10.1016/0925-8388(93)90503-F

Reference yield:

praseodymium + antimony (7440-36-0) + calcium (7440-70-2) → praseodymium monoantimonide (12066-81-8) + Ca11Sb10 + Ca3.04Pr0.95Sb3

Guidance literature:

With lead; at 999.84 ℃; for 72h; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/acs.chemmater.1c03300

Reference yield:

praseodymium + antimony (7440-36-0) → praseodymium antimonide (12066-81-8)

Guidance literature:

In neat (no solvent, solid phase); by reeact. of rare earth metal with antimony in a sealed silica tube ataround 800°C; powder XRD;

DOI:10.1016/S0038-1098(00)00113-7

upstream raw materials:

antimony

calcium

Refernces

• 1、 Borzone, G.,Borsese, A.,Zanicchi, G.,Ferro, R.. "". . p. 433 - 440. Retrieved 1982.
• 2、 Forbes, Scott,Yuan, Fang,Kosuda, Kosuke,Kolodiazhnyi, Taras,Mozharivskyj, Yurij. "Investigation of the transport properties and compositions of the Ca2RE7Pn5O5 series (RE=Pr, Sm, Gd, Dy; Pn=Sb, Bi)". . p. 148 - 154. Retrieved 2016/09/09.