2-(Tetrahydrofurfuryloxy)tetrahydropyran

Base Information

• Chemical Name: 2-(Tetrahydrofurfuryloxy)tetrahydropyran
• CAS No.: 710-14-5
• Molecular Formula: C10H18 O3
• Molecular Weight: 186.251
• Hs Code.: 2932999099
• European Community (EC) Number: 211-917-2
• NSC Number: 65618
• UNII: NAM7ZZ2HKR
• DSSTox Substance ID: DTXSID40916611
• Nikkaji Number: J99.532K
• Mol file: 710-14-5.mol

Synonyms:2-(Tetrahydrofurfuryloxy)tetrahydropyran;710-14-5;2-(oxolan-2-ylmethoxy)oxane;2-[(Oxolan-2-yl)methoxy]oxane;NAM7ZZ2HKR;2H-Pyran, tetrahydro-2-[(tetrahydrofurfuryl)oxy]-;EINECS 211-917-2;NSC-65618;2H-Pyran, tetrahydro-2-[(tetrahydro-2-furanyl)methoxy]-;94031-11-5;2H-Pyran, tetrahydro-2-((tetrahydro-2-furanyl)methoxy)-;Tetrahydro((tetrahydrofuryl)methoxy)-2H-pyran;NSC65618;UNII-NAM7ZZ2HKR;NCIOpen2_000151;SCHEMBL10354329;DTXSID40916611;Tetrahydrofurfuroxy tetrahydropyran;EINECS 301-715-3;MFCD00198008;NSC 65618;2-(Tetrahydrofurfuroxy)tetrahydropyran;AKOS025295653;2(3)-(Tetrahydrofurfuryloxy)tetrahydro-pyran;2(3)-(Tetrahydrofurfuryloxy)tetrahydropyrane;FT-0608928;(2-Oxolanylmethyl)(tetrahydro-2H-pyran-2-yl) ether;J-640049;J-800051;2-((tetrahydrofuran-2-yl)methoxy)tetrahydro-2H-pyran;2-(Tetrahydro-2-furanylmethoxy)tetrahydro-2H-pyran #;2H-Pyran,tetrahydro-2-[(tetrahydro-2-furanyl)methoxy]-;tetrahydro-2-furanylmethyl tetrahydro-2H-pyran-2-yl ether

Chemical Property of 2-(Tetrahydrofurfuryloxy)tetrahydropyran

Chemical Property:

• Vapor Pressure: 0.00376mmHg at 25°C
• Refractive Index: n20/D 1.461(lit.)
• Boiling Point: 235-238ºC
• Flash Point: 208 °F
• PSA: 27.69000
• Density: 1.03 g/mL at 25ºC(lit.)
• LogP: 1.70860
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 186.125594432
• Heavy Atom Count: 13
• Complexity: 149

Purity/Quality:

98%,99%, ^*data from raw suppliers

2(3)-(Tetrahydrofurfuryloxy)tetrahydropyran 98% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 23-24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCOC(C1)OCC2CCCO2

Technology Process of 2-(Tetrahydrofurfuryloxy)tetrahydropyran

There total 2 articles about 2-(Tetrahydrofurfuryloxy)tetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Tetrahydrofurfuryl alcohol (97-99-4) + 3,4-dihydro-2H-pyran (110-87-2) → tetrahydrofurfuryl tetrahydropyranyl ether (710-14-5)

Guidance literature:

With zirconium(IV) chloride; In dichloromethane; for 3h;

DOI:10.1080/00397910008087225

Reference yield:

→ tetrahydrofurfuryl tetrahydropyranyl ether (710-14-5)

Guidance literature:

Reference yield: 93.0%

tetrahydrofurfuryl tetrahydropyranyl ether (710-14-5) → Tetrahydrofurfuryl alcohol (97-99-4)

Guidance literature:

With methanol; zirconium(IV) chloride; at 20 ℃; for 7h;

DOI:10.1080/00397910008087225

upstream raw materials:

Tetrahydrofurfuryl alcohol

3,4-dihydro-2H-pyran

Downstream raw materials:

tetrahydrofurfuryl acetate

Tetrahydrofurfuryl alcohol

Refernces

• 1、 Duan, Zhiying,Gu, Yanlong,Deng, Youquan. "Bronsted acidic ionic liquids: Fast, mild, and efficient catalysts for solvent-free tetrahydropyranylation of alcohols". . p. 1939 - 1945. Retrieved 2007/10/03.
• 2、 Eshghi, Hossein,Shafieyoon, Parvaneh. "Phosphorus pentoxide as an efficient catalyst for the tetrahydropyranylation of alcohols under solvent-free conditions". . p. 2149 - 2152. Retrieved 2007/10/03.