4,4'-Diaminodiphenylamine Sulfate

Base Information

• Chemical Name: 4,4'-Diaminodiphenylamine Sulfate
• CAS No.: 6369-04-6
• Molecular Formula: C₁₂H₁₃N₃*H₂O₄S
• Molecular Weight: 297.335
• European Community (EC) Number: 258-748-0,228-864-6
• UNII: 02X5LJD26T
• DSSTox Substance ID: DTXSID50202037
• Wikidata: Q27231553
• Mol file: 6369-04-6.mol

Synonyms:53760-27-3;4,4'-Diaminodiphenylamine Sulfate;N1-(4-Aminophenyl)benzene-1,4-diamine sulfate;6369-04-6;4.4'-DIAMINODIPHENYLAMINESULFATE;4.4/'-Diaminodiphenylaminesulfate;EINECS 258-748-0;UNII-02X5LJD26T;02X5LJD26T;C12H15N3O4S;4,4'-diaminodiphenylamine monosulfate;4-N-(4-aminophenyl)benzene-1,4-diamine;sulfuric acid;N-(4-Aminophenyl)benzene-1,4-diamine sulphate (1:1);1,4-Benzenediamine, N-(4-aminophenyl)-, sulfate (1:1);N4-(4-aminophenyl)benzene-1,4-diamine;N1-(4-Aminophenyl)benzene-1,4-diaminesulfate;4,4'-Iminodianiline Sulfate;SCHEMBL475959;4,4'-diaminodiphenylaminsulfat;4,4-Diaminodiphenylaminesulfate;Bis(4-aminophenyl)amine Sulfate;C12H13N3.H2O4S;DTXSID50202037;4,4'-Iminodianiline sulfate salt;MFCD00013113;AKOS015915468;4,4'-Diaminodiphenylamine sulfate salt;4,4/'-Diaminodiphenylamine monosulfate;DS-5229;C12-H13-N3.H2-O4-S;P,P'-DIAMINODIPHENYLAMINE SULFATE;AC-12952;4,4'-DIAMINO DIPHENYLAMINE SULFATE;4,4'-Diaminodiphenylamine Sulfate, Hydrate;CS-0157471;D0041;FT-0617025;N11907;A829763;A829774;Q27231553;4,4'-Diaminodiphenylamine sulfate salt, technical grade, 85%;N-(4-AMINOPHENYL)-1,4-BENZENEDIAMINE SULFATE HYDRATE;1,4-BENZENEDIAMINE, N1-(4-AMINOPHENYL)-, SULFATE (1:1)

Chemical Property of 4,4'-Diaminodiphenylamine Sulfate

Chemical Property:

• Appearance/Colour: purple powder
• Boiling Point: 410.7 °C at 760 mmHg
• Flash Point: 239.2 °C
• PSA: 147.05000
• LogP: 4.25800
• Hydrogen Bond Donor Count: 5
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 2
• Exact Mass: 297.07832714
• Heavy Atom Count: 20
• Complexity: 241

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1N)NC2=CC=C(C=C2)N.OS(=O)(=O)O

Technology Process of 4,4'-Diaminodiphenylamine Sulfate

There total 3 articles about 4,4'-Diaminodiphenylamine Sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-bis-(4-nitro-phenyl)-formamide → 4,4′-diaminodiphenylamine sulfate (53760-27-3,72315-09-4,6369-04-6)

Guidance literature:

With iron; dann uebersaettigt mit Schwefelsaeure und kocht auf;

Reference yield:

N-acetyl-4,4'-dinitrodiphenylamine (106038-75-9) → 4,4′-diaminodiphenylamine sulfate (53760-27-3,72315-09-4,6369-04-6)

Guidance literature:

With iron; dann uebersaettigt mit Schwefelsaeure und kocht auf;

Reference yield:

→ 4,4′-diaminodiphenylamine sulfate (53760-27-3,72315-09-4,6369-04-6)

Guidance literature:

upstream raw materials:

N-acetyl-4,4'-dinitrodiphenylamine

Downstream raw materials:

4,4'-di(benzylthiocarbamoylamino)diphenylamine

N,N'-bis(4-aminophenyl)-1,4-benzoquinonediimine

N,N’’-bis(4’’-nitrophenyl)-4,4’-diaminodiphenylamine

N¹,N⁴-bis(4-aminophenyl)-1,4-quinonediimine

Refernces