2-{[(acetylcarbamoyl)oxy]methyl}-2,3-dimethylpentyl acetylcarbamate (non-preferred name)

Base Information

• Chemical Name: 2-{[(acetylcarbamoyl)oxy]methyl}-2,3-dimethylpentyl acetylcarbamate (non-preferred name)
• CAS No.: 25648-85-5
• Molecular Formula: C14H24 N2 O6
• Molecular Weight: 316.3502
• Mol file: 25648-85-5.mol

Synonyms:1,3-Propanediol,2-sec-butyl-2-methyl-, bis(acetylcarbamate) (8CI)

Chemical Property of 2-{[(acetylcarbamoyl)oxy]methyl}-2,3-dimethylpentyl acetylcarbamate (non-preferred name)

Chemical Property:

• Density: 1.134g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-{[(acetylcarbamoyl)oxy]methyl}-2,3-dimethylpentyl acetylcarbamate (non-preferred name)

There total 5 articles about 2-{[(acetylcarbamoyl)oxy]methyl}-2,3-dimethylpentyl acetylcarbamate (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-sec-butyl-2-methyl-propane-1,3-diol (813-60-5) → N,N'-Diacetyl-2-methyl-2-sek-butyl-1,3-dicarbamoyloxy-propan (25648-85-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Al(OiPr)3 / xylene / Heating

2: H₂SO₄

With sulfuric acid; aluminum isopropoxide; In xylene;

Reference yield:

1-methoxy-2,3-dimethyl-pentan-2-ol (3944-77-2) → N,N'-Diacetyl-2-methyl-2-sek-butyl-1,3-dicarbamoyloxy-propan (25648-85-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ion-exchange resin + form>

2: aq. Na₂CO₃

3: Al(OiPr)3 / xylene / Heating

4: H₂SO₄

With ion-exchange resin + form>; sulfuric acid; aluminum isopropoxide; sodium carbonate; In xylene;

Reference yield:

2,3-dimethylvaleraldehyde (32749-94-3,3944-76-1) → N,N'-Diacetyl-2-methyl-2-sek-butyl-1,3-dicarbamoyloxy-propan (25648-85-5)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. Na₂CO₃

2: Al(OiPr)3 / xylene / Heating

3: H₂SO₄

With sulfuric acid; aluminum isopropoxide; sodium carbonate; In xylene;

upstream raw materials:

mebutamate

acetic anhydride

2-sec-butyl-2-methyl-propane-1,3-diol

1-methoxy-2,3-dimethyl-pentan-2-ol