ZINC CAPRATE

Base Information

• Chemical Name: ZINC CAPRATE
• CAS No.: 13040-17-0
• Molecular Formula: C10H20 O2 . 1/2 Zn
• Molecular Weight: 407.909
• Mol file: 13040-17-0.mol

Synonyms:Decanoicacid, zinc salt (8CI,9CI); Zinc decanoate (7CI); Zinc caprate

Chemical Property of ZINC CAPRATE

Chemical Property:

• Vapor Pressure: 0.00355mmHg at 25°C
• Boiling Point: 269.6°Cat760mmHg
• Flash Point: 121.8°C
• PSA: 40.13000
• Density: g/cm³
• LogP: 1.87450

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ZINC CAPRATE

There total 6 articles about ZINC CAPRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-decanoic acid (334-48-5) + zinc(II) oxide → zinc(II) decanoate (13040-17-0)

Guidance literature:

In ethanol; prepn. by refluxing ZnO with excess of carboxylic acid in EtOH for about2 h; cooled; ppt. filtered off; washed (EtOH) repeatedly; collected; kept over silica gel in vac. desiccator; elem. anal.;

DOI:10.1016/j.saa.2006.11.007

Reference yield:

sodium decanoate (1002-62-6) + zinc(II) chloride (7646-85-7,24359-56-6) → zinc(II) decanoate (13040-17-0)

Guidance literature:

In ethanol; water; dissolving of sodium caprate in H2O and EtOH (50:50, v/v); slow addn. ofaq. ZnCl2 soln.; stirring for 2-3 h; pptn. in Et2O overnight; washing with H2O, EtOH and acetone; recrystn. from benzene; repeat these procedures two times;

DOI:10.1016/j.saa.2007.06.043

Reference yield:

1-decanoic acid (334-48-5) + zinc(II) hydroxide → zinc(II) decanoate (13040-17-0)

Guidance literature:

In octane; byproducts: H2O; Zn(OH)2 refluxed with 50% excess of C10H19OOH in octane; cooled slow, filtered off, washed with octane, elem. anal.;

DOI:10.1016/S0020-1693(00)85309-8

upstream raw materials:

bis(dimethylcarbamodithioato-κS,κS')zinc(II)

tetrabutylammonium decanoate

1-decanoic acid

zinc(II) nitrate

Refernces

• 1、 Suzuki, Shintaro,Ishioka, Tsutomu. "Normal mode analysis of zinc caprate (Zn)1/2O2C(CH2)8CH3". . p. 195 - 197. Retrieved 2008.
• 2、 Mirnaya,Sudovtsova,Yaremchuk,Tolochko,Lisetskii. "Phase behavior and liquid-crystal properties of transition-metal decanoates". . p. 1440 - 1443. Retrieved 2008/10/09.