Technology Process of Phosphonic acid,
[1,2-dihydroxy-1-methyl-2-(4-methyl-2-phenyl-5-thiazolyl)ethyl]-, diethyl
ester
There total 4 articles about Phosphonic acid,
[1,2-dihydroxy-1-methyl-2-(4-methyl-2-phenyl-5-thiazolyl)ethyl]-, diethyl
ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
diethyl ether; water; acetone; tert-butyl alcohol;
for 384h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / ethanol / 204 h / Heating
2: 75 percent / p-TosOH*H2O / toluene / 2 h / Heating
3: 83 percent / 4-methylmorpholine-4-oxide-monohydrate, 0.4M OsO4 / acetone; H2O; 2-methyl-propan-2-ol; diethyl ether / 384 h / Ambient temperature
With
osmium(VIII) oxide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
diethyl ether; ethanol; water; acetone; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / ethanol / 204 h / Heating
2: 75 percent / p-TosOH*H2O / toluene / 2 h / Heating
3: 83 percent / 4-methylmorpholine-4-oxide-monohydrate, 0.4M OsO4 / acetone; H2O; 2-methyl-propan-2-ol; diethyl ether / 384 h / Ambient temperature
With
osmium(VIII) oxide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
diethyl ether; ethanol; water; acetone; toluene; tert-butyl alcohol;