1-Propanone, 1-[2-(b-D-glucopyranosyloxy)-4-hydroxyphenyl]-3-(4-hydroxyphenyl)-

Base Information

• Chemical Name: 1-Propanone, 1-[2-(b-D-glucopyranosyloxy)-4-hydroxyphenyl]-3-(4-hydroxyphenyl)-
• CAS No.: 23140-78-5
• Molecular Formula: C₂₁H₂₄O₉
• Molecular Weight: 420.416
• Mol file: 23140-78-5.mol

Synonyms:Glucopyranoside,5-hydroxy-2-(p-hydroxyhydrocinnamoyl)phenyl, b-D- (8CI); Davidioside

Chemical Property of 1-Propanone, 1-[2-(b-D-glucopyranosyloxy)-4-hydroxyphenyl]-3-(4-hydroxyphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Propanone, 1-[2-(b-D-glucopyranosyloxy)-4-hydroxyphenyl]-3-(4-hydroxyphenyl)-

There total 5 articles about 1-Propanone, 1-[2-(b-D-glucopyranosyloxy)-4-hydroxyphenyl]-3-(4-hydroxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Sucrose (57-50-1) → 4,4'-dihydroxy-dihydrochalcone-2'-O-β-D-glucopyranoside (23140-78-5)

Guidance literature:

Multi-step reaction with 2 steps

1: recombinant sucrose synthase from soybean Glycine max; magnesium chloride; potassium chloride / dimethyl sulfoxide / 30 °C / pH 6.5 / Enzymatic reaction

2: magnesium chloride; potassium chloride; glycosyltransferase from pear Pyrus communis / dimethyl sulfoxide / 24 h / 30 °C / pH 7.5 / Green chemistry; Enzymatic reaction

With glycosyltransferase from pear Pyrus communis; recombinant sucrose synthase from soybean Glycine max; potassium chloride; magnesium chloride; In dimethyl sulfoxide;

DOI:10.1039/c4gc00960f

Reference yield:

phloridizin (60-81-1,6426-09-1,40816-73-7,130549-93-8,138665-98-2) → 4,4'-dihydroxy-dihydrochalcone-2'-O-β-D-glucopyranoside (23140-78-5)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium chloride; potassium chloride; glycosyltransferase from pear Pyrus communis / dimethyl sulfoxide / 6 h / 30 °C / pH 6.5 / Green chemistry; Enzymatic reaction

2: magnesium chloride; potassium chloride; glycosyltransferase from pear Pyrus communis / dimethyl sulfoxide / 24 h / 30 °C / pH 7.5 / Green chemistry; Enzymatic reaction

With glycosyltransferase from pear Pyrus communis; potassium chloride; magnesium chloride; In dimethyl sulfoxide;

DOI:10.1039/c4gc00960f

Reference yield:

recorcinol (108-46-3) → 4,4'-dihydroxy-dihydrochalcone-2'-O-β-D-glucopyranoside (23140-78-5)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / 2 h / 90 °C / Inert atmosphere

2: magnesium chloride; potassium chloride; glycosyltransferase from pear Pyrus communis / dimethyl sulfoxide / 24 h / 30 °C / pH 7.5 / Green chemistry; Enzymatic reaction

With boron trifluoride diethyl etherate; glycosyltransferase from pear Pyrus communis; potassium chloride; magnesium chloride; In dimethyl sulfoxide; 1: |Friedel-Crafts Acylation;

DOI:10.1039/c4gc00960f

upstream raw materials:

Sucrose

UDP-glucose

davidigenin

phloridizin

Refernces