Technology Process of Carbamic acid, [3-bromo-5-(1-methylethyl)phenyl]-, 1,1-dimethylethyl ester
There total 3 articles about Carbamic acid, [3-bromo-5-(1-methylethyl)phenyl]-, 1,1-dimethylethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) magnesium, iodine, 2.) hydrochloric acid (3M) / 1.) ether, reflux, 2.) ether, overnight
2: thionyl chloride / 5 h / Heating
3: 1.) sodium azide (20percent) / 1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h
With
hydrogenchloride; thionyl chloride; sodium azide; iodine; magnesium;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / 5 h / Heating
2: 1.) sodium azide (20percent) / 1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h
With
thionyl chloride; sodium azide;
- Guidance literature:
-
With
sodium azide;
Yield given. Multistep reaction;
1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h;