Antimony sulfide

Base Information

• Chemical Name: Antimony sulfide
• CAS No.: 1317-86-8
• Molecular Formula: S₀Sb₀
• Molecular Weight: 70.6301
• UN Number: 1549
• DSSTox Substance ID: DTXSID90152961
• Mol file: 1317-86-8.mol

Synonyms:Antimony sulfide;Sulfanylideneantimony;12627-52-0;Vitreous antimony;Antimony sulfide, solid;DTXSID90152961;AKOS030228260

Chemical Property of Antimony sulfide

Chemical Property:

• Density: 4.570
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 152.87588
• Heavy Atom Count: 2
• Complexity: 2
• Transport DOT Label: Poison

Purity/Quality:

99%, ^*data from raw suppliers

STIBNITE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: S=[Sb]

Technology Process of Antimony sulfide

There total 9 articles about Antimony sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lead(II) sulfide + antimony(III) sulfide → lead (7439-92-1) + antimony (7440-36-0) + antimony subsulfide (1315-04-4,1317-86-8) + sulfur (7704-34-9)

Guidance literature:

in gaseous phase;

Reference yield:

[Sb2Cl5(1-(naphthalene-2-ylmethylene)thiosemicarbazide)]Cl*4H2O → antimony (7440-36-0) + antimony subsulfide (1315-04-4,1317-86-8) + pyrographite (7440-44-0)

Guidance literature:

In neat (no solvent); byproducts: H2O, Cl2, C11H11N3S; heating up to 1500°C under N2, heating rate of 10°C/min; TG;

DOI:10.1016/j.saa.2011.06.045

Reference yield:

antimony (7440-36-0) + sulfur (7704-34-9) → Sb0.45S0.55 (1317-86-8)

Guidance literature:

In neat (no solvent); fusion of the elementary compds. in thinwalled quartz ampuls evacuated to a pressure of 133 P at the 3-4 g quantity, homogenization temp. of the melt: depending on composition between 850 - 1100 ° K;

upstream raw materials:

antimony

sulfur

Refernces