3,10-Perylenedicarboxylic acid

Base Information

• Chemical Name: 3,10-Perylenedicarboxylic acid
• CAS No.: 113659-72-6
• Molecular Formula: C22H12O4
• Molecular Weight: 340.335
• Mol file: 113659-72-6.mol

Synonyms:

Chemical Property of 3,10-Perylenedicarboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,10-Perylenedicarboxylic acid

There total 1 articles about 3,10-Perylenedicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride (128-69-8) → 3,10-perylenedicarboxylic acid (113659-72-6) + 3,9-perylene dicarboxylic acid (6364-19-8)

Guidance literature:

With potassium hydroxide; at 198 ℃; for 36h; under 15001.5 Torr;

Reference yield:

3,10-perylenedicarboxylic acid (113659-72-6) → PERYLENE (198-55-0)

Guidance literature:

With ammonia; at 250 - 260 ℃; im Autoklaven;

Reference yield:

3,10-perylenedicarboxylic acid (113659-72-6) + 3,9-perylene dicarboxylic acid (6364-19-8) → perylene-3,10-dicarbonyl chloride (923584-56-9) + perylene-3,9-dicarbonyl chloride (47477-48-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In toluene; at 20 - 110 ℃; for 5.25h;

upstream raw materials:

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

Downstream raw materials:

PERYLENE

perylene-3,10-dicarbonyl chloride

perylene-3,9-dicarbonyl chloride

Refernces