4-Nitro-o-phenylenediamine hydrochloride

Base Information

• Chemical Name: 4-Nitro-o-phenylenediamine hydrochloride
• CAS No.: 53209-19-1
• Molecular Formula: C₆H₇N₃O₂*ClH
• Molecular Weight: 189.601
• Hs Code.: 2921590090
• European Community (EC) Number: 258-429-6
• UNII: R6FRD37482
• DSSTox Substance ID: DTXSID70201289
• Wikidata: Q27287851
• Mol file: 53209-19-1.mol

Synonyms:53209-19-1;4-nitrobenzene-1,2-diamine hydrochloride;4-Nitro-1,2-phenylenediamine Monohydrochloride;4-Nitro-o-phenylenediamine hydrochloride;CCRIS 9089;4-Nitro-o-phenylenediamine monohydrochloride;4-Nitrobenzene-1,2-diamine monohydrochloride;EINECS 258-429-6;4-nitrobenzene-1,2-diamine;hydrochloride;UNII-R6FRD37482;R6FRD37482;4-Nitro-1,2-phenylenediamine monoHCl;SCHEMBL970606;DTXSID70201289;MFCD00043273;AKOS016846129;4-nitrobenzene-1,2-diaminehydrochloride;AS-64534;LS-188619;CS-0205232;FT-0619181;1,2-Diamino-4-nitrobenzene Monohydrochloride;4-NITRO-O-PHENYLENEDIAMINE HCL [INCI];D88565;A829445;O-PHENYLENEDIAMINE, 4-NITRO-, HYDROCHLORIDE;4-Nitro-1,2-benzenediamine hydrochloride, AldrichCPR;Q27287851;1,2-BENZENEDIAMINE, 4-NITRO-, MONOHYDROCHLORIDE;1,2-BENZENEDIAMINE, 4-NITRO-, HYDROCHLORIDE (1:1)

Chemical Property of 4-Nitro-o-phenylenediamine hydrochloride

Chemical Property:

• Vapor Pressure: 2.68E-07mmHg at 25°C
• Boiling Point: 421.1 °C at 760 mmHg
• Flash Point: 208.5 °C
• PSA: 97.86000
• LogP: 3.24680
• Solubility.: almost transparency in 1mol/L HCl
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 189.0305042
• Heavy Atom Count: 12
• Complexity: 156

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Nitro-1,2-phenylenediamineMonohydrochloride ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22-36/37/38-43
• Safety Statements: 26-36/37/39-36/37

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1[N+](=O)[O-])N)N.Cl

Technology Process of 4-Nitro-o-phenylenediamine hydrochloride

There total 1 articles about 4-Nitro-o-phenylenediamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Nitrophenylene-1,2-diamine (99-56-9) → 2-amino-5-nitroanilinium chloride (6219-77-8,53209-19-1)

Guidance literature:

With hydrogenchloride; In ethanol;

DOI:10.1107/S2053229614013485

Reference yield:

acetone (67-64-1) + 4-nitro-o-phenylenediamine dihydrochloride (6219-77-8,53209-19-1) → N1,N2-Diisopropylidene-4-nitro-benzene-1,2-diamine

Guidance literature:

With sodium hydroxide; Heating;

upstream raw materials:

4-Nitrophenylene-1,2-diamine

Refernces